1,3-Diethyltriazene

Base Information

• Chemical Name: 1,3-Diethyltriazene
• CAS No.: 63980-20-1
• Molecular Formula: C4H11 N3
• Molecular Weight: 101.151
• UNII: I93E81I3BD
• DSSTox Substance ID: DTXSID30213848
• Nikkaji Number: J408.677E
• Wikidata: Q27280592
• Mol file: 63980-20-1.mol

Synonyms:1,3-diethyltriazene

Chemical Property of 1,3-Diethyltriazene

Chemical Property:

• Vapor Pressure: 25.2mmHg at 25°C
• Refractive Index: 1.4750 (estimate)
• Boiling Point: 109.1°C at 760 mmHg
• PKA: 9.70±0.70(Predicted)
• Flash Point: 19.8°C
• PSA: 36.75000
• Density: 0.92g/cm³
• LogP: 1.37390
• XLogP3: 1.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 101.095297364
• Heavy Atom Count: 7
• Complexity: 50.9

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCNN=NCC

Technology Process of 1,3-Diethyltriazene

There total 2 articles about 1,3-Diethyltriazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyllithium (811-49-4) + ethyl azide (871-31-8) → 1,3-diethyltriazene (63980-20-1)

Guidance literature:

DOI:10.1021/ja00273a029

Reference yield:

ethyl bromide (74-96-4) + ethyl azide (871-31-8) → 1,3-Diethyltriazene (63980-20-1)

Guidance literature:

With magnesium; Yield given. Multistep reaction; 1.) ether, 2.) ether, 0 deg C, 1h;

Reference yield:

1,3-diethyltriazene (63980-20-1) → ethanol (64-17-5) + ethylamine (75-04-7,85404-22-4)

Guidance literature:

With phosphate buffer; In water; at 25 ℃; Rate constant; Mechanism; further buffer (different pH), and different concentrations;

DOI:10.1021/ja00273a029

upstream raw materials:

ethyl bromide

ethyl azide

ethyllithium

Downstream raw materials:

ethanol

ethylamine

Refernces

• 1、 Smith, Richard H.,Michejda, Christopher J.. "Synthesis of Triazenes: Efficient Preparation of the Simplest Di- and Trialkyltriazenes and a Novel 3-Acyl-1,3-dialkyltriazene". . p. 476 - 477. Retrieved 2007/10/02.