1,5-Dichloro-2-(1-methylethoxy)-4-nitrobenzene

Base Information

• Chemical Name: 1,5-Dichloro-2-(1-methylethoxy)-4-nitrobenzene
• CAS No.: 41200-97-9
• Molecular Formula: C9H9 Cl2 N O3
• Molecular Weight: 250.081
• Hs Code.: 2909309090
• European Community (EC) Number: 255-259-4
• DSSTox Substance ID: DTXSID50194125
• Nikkaji Number: J30.018G
• Wikidata: Q83066880
• Mol file: 41200-97-9.mol

Synonyms:41200-97-9;1,5-dichloro-2-isopropoxy-4-nitrobenzene;1,5-Dichloro-2-(1-methylethoxy)-4-nitrobenzene;1,5-dichloro-2-nitro-4-propan-2-yloxybenzene;EINECS 255-259-4;2,4-Dichloro-5-isopropoxynitrobenzene;2,4-Dichloro-5-nitrophenylIsopropyl-d7Ether;EC 255-259-4;2,4-Dichloro-5-nitrophenyl Isopropyl Ether;DTXSID50194125;AKOS016006622;A6837;FT-0655103;1,3-Dichloro-4-(1-methylethoxy)-6-nitrobenzene;W-110947

Chemical Property of 1,5-Dichloro-2-(1-methylethoxy)-4-nitrobenzene

Chemical Property:

• Vapor Pressure: 0.000191mmHg at 25°C
• Boiling Point: 338.6°Cat760mmHg
• Flash Point: 158.6°C
• PSA: 55.05000
• Density: 1.369g/cm³
• LogP: 4.21200
• Storage Temp.: 2-8°C
• Solubility.: Chloroform (Sparingly), DMSO (Slightly), Methanol (Slightly)
• XLogP3: 3.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 248.9959485
• Heavy Atom Count: 15
• Complexity: 232

Purity/Quality:

99.9% ^*data from raw suppliers

2,4-Dichloro-5-nitrophenylIsopropylEther ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)OC1=C(C=C(C(=C1)[N+](=O)[O-])Cl)Cl
• Uses: 2,4-Dichloro-5-nitrophenyl Isopropyl Ether is a 2,4-disubstituted-5-nitrophenol used in the synthesis of the herbicide Oxadiazon.

Technology Process of 1,5-Dichloro-2-(1-methylethoxy)-4-nitrobenzene

There total 3 articles about 1,5-Dichloro-2-(1-methylethoxy)-4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-dichloro-5-nitrophenol? (39489-77-5) + isopropyl bromide (75-26-3) → 2,4-dichloro-5-isopropoxy-1-nitrobenzene (41200-97-9)

Guidance literature:

With potassium carbonate; ortho-cresol; In N,N-dimethyl-formamide; at 40 - 50 ℃; Large scale;

Reference yield:

2,4-dichloro-5-nitrophenol? (39489-77-5) → 2,4-dichloro-5-isopropoxy-1-nitrobenzene (41200-97-9)

Guidance literature:

Reference yield:

→ 2,4-dichloro-5-isopropoxy-1-nitrobenzene (41200-97-9)

Guidance literature:

entspr. Phenol, Isopropylbromid;

upstream raw materials:

2,4-dichloro-5-nitrophenol?

isopropyl bromide

Downstream raw materials:

2-(2,4-dichloro-5-isopropoxyphenyl)-1,2,4,5,6,7-hexahydro-3H-indazol-3-one

2,4-dichloro-5-(1-methylethoxy)phenylhydrazine

2,4-dichloro-5-isopropoxyaniline

Refernces

• 1、 Ando, Iwao,Ohtsuka, Toshikazu,Miki, Nobuo,Takahashi, Toshio,Hayase, Yoshio,Hayashi, Yoshiyuki. "Synthesis and Biological Activity of Cyclic Imide Derivatives and Related Compounds". . p. 2001 - 2004. Retrieved 2007/10/02.