Dodecan-1-amine;hydron;chloride

Base Information

• Chemical Name: Dodecan-1-amine;hydron;chloride
• CAS No.: 929-73-7
• Molecular Formula: C12H27 N . Cl H
• Molecular Weight: 221.814
• Hs Code.: 29211999
• Mol file: 929-73-7.mol

Synonyms:SCHEMBL8994696

Chemical Property of Dodecan-1-amine;hydron;chloride

Chemical Property:

• Appearance/Colour: white powder
• Melting Point: 186-188°C
• Boiling Point: 258.6°Cat760mmHg
• Flash Point: 100.4°C
• PSA: 26.02000
• Density: g/cm³
• LogP: 5.36830
• Solubility.: soluble in Methanol
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 10
• Exact Mass: 221.1910276
• Heavy Atom Count: 14
• Complexity: 81.2

Purity/Quality:

98%,99%, ^*data from raw suppliers

Dodecylamine Hydrochloride ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 36/37/38-22
• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: [H+].CCCCCCCCCCCCN.[Cl-]

Technology Process of Dodecan-1-amine;hydron;chloride

There total 6 articles about Dodecan-1-amine;hydron;chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

undecyl cyanide (2437-25-4) → dodecylammonium chloride (929-73-7)

Guidance literature:

undecyl cyanide; With titanium(IV) isopropylate; 1,1,3,3-Tetramethyldisiloxane; In toluene; at 60 ℃; for 24h; Inert atmosphere;

With hydrogenchloride; In water; at 20 ℃;

DOI:10.1016/j.tetlet.2009.09.164

Reference yield: 95.0%

dodecyl azide (13733-78-3) → dodecylammonium chloride (929-73-7)

Guidance literature:

With propan-1-ol; 2,2'-azobis(isobutyronitrile); bis(tri-n-butyltin)oxide; at 80 ℃;

DOI:10.1021/jo9721958

Reference yield: 85.0%

n-Dodecylamine (124-22-1) → dodecylammonium chloride (929-73-7)

Guidance literature:

With hydrogenchloride; In methanol; diethyl ether;

upstream raw materials:

dodecyl azide

N-trityldodecan-1-amine

n-Dodecylamine

undecyl cyanide

Downstream raw materials:

N-dodecyl srearamide

2-(dodecylamino)benzoic acid

trimethyldodecylammonium chloride

C₂₃H₄₀⁽¹³¹⁾INO₂

Refernces

• 1、 El-Shamy, Omnia A. A.,Habib, Amr O.,Mohamed, Dalia E.,Badawi, Abdelfattah M.. "Synthesis, Characterization, Surface, and Thermodynamic Studies of Alkyl Tetrachloroferrates: Performance Evaluation of Their Nanostructures as Biocides". . p. 215 - 223. Retrieved 2019/11/03.
• 2、 Weber, Stefan,Veiros, Luis F.,Kirchner, Karl. "Old Concepts, New Application – Additive-Free Hydrogenation of Nitriles Catalyzed by an Air Stable Alkyl Mn(I) Complex". supporting information. p. 5412 - 5420. Retrieved 2019/11/13.