6-<2-<<(Aminoiminomethyl)hydrazono>methyl>phenoxy>hexanoic acid hemisulfate

Base Information

• Chemical Name: 6-<2-<<(Aminoiminomethyl)hydrazono>methyl>phenoxy>hexanoic acid hemisulfate
• CAS No.: 147452-31-1
• Molecular Formula: 2C₁₄H₂₀N₄O₃*H₂O₄S
• Molecular Weight: 682.755
• Mol file: 147452-31-1.mol

Synonyms:6-<2-<<(Aminoiminomethyl)hydrazono>methyl>phenoxy>hexanoic acid hemisulfate

Chemical Property of 6-<2-<<(Aminoiminomethyl)hydrazono>methyl>phenoxy>hexanoic acid hemisulfate

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-<2-<<(Aminoiminomethyl)hydrazono>methyl>phenoxy>hexanoic acid hemisulfate

There total 3 articles about 6-<2-<<(Aminoiminomethyl)hydrazono>methyl>phenoxy>hexanoic acid hemisulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

aminoguanidine sulfate (996-19-0,1068-42-4) + Ethyl 6-<2-(formyl)phenoxy>hexanoate (146940-58-1) → 6-<2-<<(Aminoiminomethyl)hydrazono>methyl>phenoxy>hexanoic acid hemisulfate (147452-31-1)

Guidance literature:

With sulfuric acid; at 80 ℃; for 4h;

DOI:10.1002/ardp.19923251206

Reference yield:

6-bromo-hexanoic acid ethyl ester (25542-62-5) → 6-<2-<<(Aminoiminomethyl)hydrazono>methyl>phenoxy>hexanoic acid hemisulfate (147452-31-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 22 percent / K₂CO₃ / acetone / 3 h / 80 °C

2: 65 percent / 2 N H₂SO₄ / 4 h / 80 °C

With sulfuric acid; potassium carbonate; In acetone;

DOI:10.1002/ardp.19923251206

Reference yield:

salicylaldehyde (90-02-8) → 6-<2-<<(Aminoiminomethyl)hydrazono>methyl>phenoxy>hexanoic acid hemisulfate (147452-31-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 22 percent / K₂CO₃ / acetone / 3 h / 80 °C

2: 65 percent / 2 N H₂SO₄ / 4 h / 80 °C

With sulfuric acid; potassium carbonate; In acetone;

DOI:10.1002/ardp.19923251206

upstream raw materials:

aminoguanidine sulfate

Ethyl 6-<2-(formyl)phenoxy>hexanoate

6-bromo-hexanoic acid ethyl ester

salicylaldehyde

Refernces