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phenylstibane

Base Information Edit
  • Chemical Name:phenylstibane
  • CAS No.:58266-50-5
  • Molecular Formula:C6H7Sb
  • Molecular Weight:200.872
  • Hs Code.:
  • Mol file:58266-50-5.mol
phenylstibane

Synonyms:phenylstibane

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Chemical Property of phenylstibane Edit
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Technology Process of phenylstibane

There total 12 articles about phenylstibane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With lithium borohydride; In diethyl ether; byproducts: B2H6; by addn. soln. of C6H5SbCl2 in ether dropwise to ethereal suspension of LiBH4 at -60°C; after evapn. of B2H6 concn. of soln. at -40°C; fractionated condensation at 1E-4 - 1E-5 Torr in cooled traps; repeated condensations;
Guidance literature:
With methanol; In diethyl ether; To stibane compound in Et2O is added under Ar methanol at -50°C, the soln. is stirred for 0.5 h.; removal of volatiles under vac.;
Guidance literature:
With lithium borohydride; In diethyl ether; with 2.5-fold excess of LiBH4, at -50°C;
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