Amylene dichloride

Base Information

• Chemical Name: Amylene dichloride
• CAS No.: 507-45-9
• Molecular Formula: C5H10 Cl2
• Molecular Weight: 141.04
• Hs Code.: 2903199000
• European Community (EC) Number: 827-520-8
• UNII: 26110Z568S
• DSSTox Substance ID: DTXSID70862071
• Nikkaji Number: J110.569H
• Wikidata: Q27254028
• Mol file: 507-45-9.mol

Synonyms:AMYLENE DICHLORIDE;2,3-Dichloro-2-methylbutane;507-45-9;Butane, 2,3-dichloro-2-methyl-;UNII-26110Z568S;BUTANE,2,3-DICHLORO-2-METH;26110Z568S;DL-AMYLENE DICHLORIDE;C5H10Cl2;TERT-AMYLENE DICHLORIDE;2,3-dichloro-2-methyl-butane;AMYLENE DICHLORIDE [MI];SCHEMBL12855564;DTXSID70862071;TXTORVZCRUFBBO-UHFFFAOYSA-N;Butene, 2,3-dichloro-2-methyl-;AMYLENE DICHLORIDE DL-FORM [MI];EN300-2148113;Q27254028

Chemical Property of Amylene dichloride

Chemical Property:

• Vapor Pressure: 8.53mmHg at 25°C
• Melting Point: -75.05°C (estimate)
• Refractive Index: 1.4600
• Boiling Point: 138°Cat760mmHg
• Flash Point: 29.5°C
• PSA: 0.00000
• Density: 1.05g/cm³
• LogP: 2.63110
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 140.0159557
• Heavy Atom Count: 7
• Complexity: 59.1

Purity/Quality:

98%min ^*data from raw suppliers

AMYLENE DICHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C(C)(C)Cl)Cl

Technology Process of Amylene dichloride

There total 10 articles about Amylene dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

BPA (80-05-7) → 2,6-Dichlorophenol (87-65-0) + 2,3-dichloro-2-methylbutane (507-45-9) + 2,6-dichloro-1,4-benzoquinone (697-91-6) + 2,2-bis(3-chloro-4-hydroxyphenyl)propane (79-98-1) + Tetrachlorobisphenol A (79-95-8) + 1,3-Dichloroacetone (534-07-6) + 2,4,6-Trichlorophenol (88-06-2,67471-29-8)

Guidance literature:

With sodium chloride; In water; at 20 ℃; Concentration; Kinetics; Electrolysis;

DOI:10.1016/j.electacta.2016.11.086

Reference yield:

methylbutane (78-78-4) + 14-phenyl-14H-dibenzo[a.j]xanthene (36441-29-9) → 1,3-dichloro-3-methylbutane (624-96-4) + 1-chloro-2-methylbutane (616-13-7) + 2,3-dichloro-2-methylbutane (507-45-9) + 1,4-dichloro-2-methylbutane (623-34-7)

Guidance literature:

at 18 - 20 ℃; Produkt 5: 2.3.3.-Trichlor-2-methyl-butan;

Reference yield:

neopentyl iodide (15501-33-4) → 2-methyl-2-butylchloride (594-36-5) + 2,3-dichloro-2-methylbutane (507-45-9)

Guidance literature:

With chlorine; Petroleum ether; at -78 ℃;

DOI:10.1021/ja01626a029

upstream raw materials:

neopentyl iodide

methylbutane

14-phenyl-14H-dibenzo[a.j]xanthene

3-methyl-but-1-yne

Downstream raw materials:

1-chloro-3-methylbut-2-ene

3-chloro-2-methylbut-1-ene

isoprene

3,3-dichloro-2-methyl-but-1-ene

Refernces

• 1、 Stammann, Guenter,Griesbaum, Karl. "Reactions of Hydrogen Chloride with 3-Methyl-1-butyne: Cycloaddition and Rearrangement Reactions via Vinyl Cations". . p. 598 - 606. Retrieved 2007/10/02.