C₃₇H₂₄N₂

Base Information

• Chemical Name: C₃₇H₂₄N₂
• CAS No.: 1262867-02-6
• Molecular Formula: C₃₇H₂₄N₂
• Molecular Weight: 496.611
• Mol file: 1262867-02-6.mol

Synonyms:C₃₇H₂₄N₂

Chemical Property of C₃₇H₂₄N₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₃₇H₂₄N₂

There total 4 articles about C₃₇H₂₄N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.21%

C25H15ClN2 (1262867-01-5) + 4-biphenylboronic acid (5122-94-1) → C37H24N2 (1262867-02-6)

Guidance literature:

With potassium phosphate; tri-tert-butyl phosphine; palladium diacetate; In 1,4-dioxane; toluene; at 100 ℃; for 5h;

Reference yield:

1-Naphthylboronic acid (13922-41-3) → C37H24N2 (1262867-02-6)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 4 h / 100 °C

2: triethyl phosphite / dichlorobenzene, 1,2- / 12 h / 150 °C

3: caesium carbonate / copper(l) iodide; trans-1,2-cyclohexanediamine / dichlorobenzene, 1,2- / 12 h / 180 °C

4: potassium phosphate / palladium diacetate; tri-tert-butyl phosphine / toluene; 1,4-dioxane / 5 h / 100 °C

With potassium phosphate; potassium carbonate; caesium carbonate; triethyl phosphite; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium diacetate; trans-1,2-cyclohexanediamine; In 1,4-dioxane; dichlorobenzene, 1,2-; ethanol; toluene;

Reference yield:

1-(2-nitrophenyl)naphthalene (5415-59-8) → C37H24N2 (1262867-02-6)

Guidance literature:

Multi-step reaction with 3 steps

1: triethyl phosphite / dichlorobenzene, 1,2- / 12 h / 150 °C

2: caesium carbonate / copper(l) iodide; trans-1,2-cyclohexanediamine / dichlorobenzene, 1,2- / 12 h / 180 °C

3: potassium phosphate / palladium diacetate; tri-tert-butyl phosphine / toluene; 1,4-dioxane / 5 h / 100 °C

With potassium phosphate; caesium carbonate; triethyl phosphite; copper(l) iodide; tri-tert-butyl phosphine; palladium diacetate; trans-1,2-cyclohexanediamine; In 1,4-dioxane; dichlorobenzene, 1,2-; toluene;

upstream raw materials:

benzo[c]carbazole

1-Naphthylboronic acid

C₂₅H₁₅ClN₂

4-biphenylboronic acid

Downstream raw materials:

C₃₇H₂₃BrN₂

Refernces