2-Fluoro-4-dimethylaminoazobenzene

Base Information

• Chemical Name: 2-Fluoro-4-dimethylaminoazobenzene
• CAS No.: 321-25-5
• Molecular Formula: C₁₄H₁₄FN₃
• Molecular Weight: 243.284
• DSSTox Substance ID: DTXSID901039097
• Nikkaji Number: J55.366B
• Mol file: 321-25-5.mol

Synonyms:2-Fluoro-4-dimethylaminoazobenzene;321-25-5;BRN 1820356;N,N-Dimethyl-2-fluoro-4-phenylazoaniline;ANILINE, N,N-DIMETHYL-2-FLUORO-4-PHENYLAZO-;4-16-00-00522 (Beilstein Handbook Reference);2-Fluoro-N,N-dimethyl-4-(phenylazo)aniline;SCHEMBL3498925;DTXSID901039097;LS-19747;Benzenamine, 2-fluoro-N,N-dimethyl-4-(2-phenyldiazenyl)-

Chemical Property of 2-Fluoro-4-dimethylaminoazobenzene

Chemical Property:

• Vapor Pressure: 9.91E-06mmHg at 25°C
• Boiling Point: 372°C at 760 mmHg
• Flash Point: 178.8°C
• PSA: 27.96000
• Density: 1.09g/cm³
• LogP: 4.30710
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 243.11717562
• Heavy Atom Count: 18
• Complexity: 274

Purity/Quality:

98%min ^*data from raw suppliers

N,N-DIMETHYL-2-FLUORO-4-PHENYLAZOANILINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=C(C=C(C=C1)N=NC2=CC=CC=C2)F

Technology Process of 2-Fluoro-4-dimethylaminoazobenzene

There total 5 articles about 2-Fluoro-4-dimethylaminoazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-fluoro-N,N-dimethylaniline (393-56-6) → 2-fluoro-N,N-dimethyl-4-phenylazo-aniline (321-25-5)

Guidance literature:

ueber mehrere Stufen;

Reference yield:

2-Fluoroaniline (348-54-9) → trans-3-Fluor-4-dimethylamino-azobenzol (321-25-5)

Guidance literature:

Multi-step reaction with 4 steps

1: aq. NaOH

2: (i) aq. HCl, (ii) aq. NaNO₂, (iii) /BRN= 2078394/, aq. HCl

3: Al, aq. HCl

4: AcOH

With hydrogenchloride; sodium hydroxide; acetic acid; aluminium;

Reference yield:

2-fluoro-N,N-dimethylaniline (393-56-6) → trans-3-Fluor-4-dimethylamino-azobenzol (321-25-5)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) aq. HCl, (ii) aq. NaNO₂, (iii) /BRN= 2078394/, aq. HCl

2: Al, aq. HCl

3: AcOH

With hydrogenchloride; acetic acid; aluminium;

upstream raw materials:

2-fluoro-N₁,N₁-dimethylbenzene-1,4-diamine

Nitrosobenzene

2-Fluoroaniline

2-fluoro-N,N-dimethylaniline