Technology Process of 3-(p-anisyl)-2,2,3-trimethylbutanal
There total 4 articles about 3-(p-anisyl)-2,2,3-trimethylbutanal which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridinium chlorochromate;
In
dichloromethane;
for 1.25h;
DOI:10.1021/ja00211a034
- Guidance literature:
-
Multi-step reaction with 4 steps
1: boron tribromide / CHCl3 / 10 h
2: 24.1 percent / KOH, KMnO4 / tetrahexylammonium bromide / H2O; benzene / 18 h / Heating
3: 97.4 percent / lithium aluminium hydride / tetrahydrofuran / 1.) ice cooling, 23 h; 2.) reflux, 1.5 h
4: 85 percent / pyridinium chlorochromate / CH2Cl2 / 1.25 h
With
potassium hydroxide; potassium permanganate; lithium aluminium tetrahydride; boron tribromide; pyridinium chlorochromate;
tetrahexylammonium bromide;
In
tetrahydrofuran; dichloromethane; chloroform; water; benzene;
DOI:10.1021/ja00211a034
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 24.1 percent / KOH, KMnO4 / tetrahexylammonium bromide / H2O; benzene / 18 h / Heating
2: 97.4 percent / lithium aluminium hydride / tetrahydrofuran / 1.) ice cooling, 23 h; 2.) reflux, 1.5 h
3: 85 percent / pyridinium chlorochromate / CH2Cl2 / 1.25 h
With
potassium hydroxide; potassium permanganate; lithium aluminium tetrahydride; pyridinium chlorochromate;
tetrahexylammonium bromide;
In
tetrahydrofuran; dichloromethane; water; benzene;
DOI:10.1021/ja00211a034
