Technology Process of 2,3,3-Triphenylacrylonitrile
There total 26 articles about 2,3,3-Triphenylacrylonitrile which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Triphenylvinyl bromide;
With
copper(I) oxide; oxygen; triphenylphosphine;
In
1-methyl-pyrrolidin-2-one;
Schlenk technique;
Sealed tube;
ethyl 2-cyanoacetate;
With
silver nitrate; acetic acid;
In
1-methyl-pyrrolidin-2-one;
at 130 ℃;
for 18h;
Schlenk technique;
Sealed tube;
DOI:10.1039/c7nj03405a
- Guidance literature:
-
With
palladium diacetate; sodium carbonate;
In
N,N-dimethyl acetamide;
at 120 ℃;
for 5h;
Inert atmosphere;
DOI:10.1021/ol703018t
- Guidance literature:
-
phenylacetonitrile;
With
sodium hydride;
In
tetrahydrofuran; mineral oil;
at 40 ℃;
for 2h;
benzophenone;
In
tetrahydrofuran; mineral oil;
for 6h;
Reflux;
DOI:10.1039/c3ra23188g
