[1-Phenyl-1-(2-phenylamino-phenyl)-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

Base Information

• Chemical Name: [1-Phenyl-1-(2-phenylamino-phenyl)-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester
• CAS No.: 209412-72-6
• Molecular Formula: C₂₅H₂₆N₂O₄
• Molecular Weight: 418.492
• Mol file: 209412-72-6.mol

Synonyms:[1-Phenyl-1-(2-phenylamino-phenyl)-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

Chemical Property of [1-Phenyl-1-(2-phenylamino-phenyl)-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [1-Phenyl-1-(2-phenylamino-phenyl)-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

There total 3 articles about [1-Phenyl-1-(2-phenylamino-phenyl)-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenyl(2-(phenylamino)phenyl)methanone (23699-69-6) → [1-Phenyl-1-(2-phenylamino-phenyl)-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester (209412-72-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 85 percent / NH₂OH*HCl, pyridine / ethanol / 1 h / Heating

2: 69 percent / NaOH / H₂O / 16 h / Heating

3: 1.) CDI / 1.) THF, r.t., 1 h, 2.) THF, light petroleum, 0-5 deg C, 4 h

With pyridine; sodium hydroxide; hydroxylamine hydrochloride; 1,1'-carbonyldiimidazole; In ethanol; water;

DOI:10.1039/a800868j

Reference yield:

Phenyl-(2-phenylamino-phenyl)-methanone oxime (209412-49-7) → [1-Phenyl-1-(2-phenylamino-phenyl)-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester (209412-72-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / NaOH / H₂O / 16 h / Heating

2: 1.) CDI / 1.) THF, r.t., 1 h, 2.) THF, light petroleum, 0-5 deg C, 4 h

With sodium hydroxide; 1,1'-carbonyldiimidazole; In water;

DOI:10.1039/a800868j

Reference yield:

tert.-butylhydroperoxide (75-91-2) + [1-Phenyl-1-(2-phenylamino-phenyl)-meth-(E)-ylideneaminooxy]-acetic acid (209412-60-2) → [1-Phenyl-1-(2-phenylamino-phenyl)-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester (209412-72-6)

Guidance literature:

With 1,1'-carbonyldiimidazole; Yield given. Multistep reaction; 1.) THF, r.t., 1 h, 2.) THF, light petroleum, 0-5 deg C, 4 h;

DOI:10.1039/a800868j

upstream raw materials:

tert.-butylhydroperoxide

[1-Phenyl-1-(2-phenylamino-phenyl)-meth-(E)-ylideneaminooxy]-acetic acid

phenyl(2-(phenylamino)phenyl)methanone

Phenyl-(2-phenylamino-phenyl)-methanone oxime

Downstream raw materials:

9-phenylacridine

Refernces