4,4-diethyl-1-phenylthiosemicarbazide

Base Information

• Chemical Name: 4,4-diethyl-1-phenylthiosemicarbazide
• CAS No.: 27421-93-8
• Molecular Formula: C₁₁H₁₇N₃S
• Molecular Weight: 223.342
• Mol file: 27421-93-8.mol

Synonyms:4,4-diethyl-1-phenylthiosemicarbazide

Chemical Property of 4,4-diethyl-1-phenylthiosemicarbazide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 4,4-diethyl-1-phenylthiosemicarbazide

There total 1 articles about 4,4-diethyl-1-phenylthiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethylamine (109-89-7) + methyl 2-phenylhydrazinecarbodithioate (50878-38-1) → 4,4-diethyl-1-phenylthiosemicarbazide (27421-93-8)

Guidance literature:

Reference yield:

4,4-diethyl-1-phenylthiosemicarbazide (27421-93-8) → N,N-diethyl-(2-phenyldiazenyl)thioformamide (39484-81-6)

Guidance literature:

With oxygen; diethylamine; at 20 ℃; for 24h;

DOI:10.1021/ma047635t

Reference yield:

phosgene (75-44-5) + 4,4-diethyl-1-phenylthiosemicarbazide (27421-93-8) → 5-diethylamino-3-phenyl-3H-[1,3,4]thiadiazol-2-one (27434-17-9)

Guidance literature:

upstream raw materials:

diethylamine

methyl 2-phenylhydrazinecarbodithioate

Downstream raw materials:

5-diethylamino-3-phenyl-3H-[1,3,4]thiadiazol-2-one

N,N-diethyl-(2-phenyldiazenyl)thioformamide

Refernces