Biacetyl Benzoylhydrazone Phenylhydrazone

Base Information

• Chemical Name: Biacetyl Benzoylhydrazone Phenylhydrazone
• CAS No.: 31400-24-5
• Molecular Formula: C₁₇H₁₈N₄O
• Molecular Weight: 294.356
• Mol file: 31400-24-5.mol

Synonyms:Biacetyl Benzoylhydrazone Phenylhydrazone

Chemical Property of Biacetyl Benzoylhydrazone Phenylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of Biacetyl Benzoylhydrazone Phenylhydrazone

There total 1 articles about Biacetyl Benzoylhydrazone Phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

biacetyl monobenzoyl hydrazone (55590-53-9) + phenylhydrazine (100-63-0) → Biacetyl Benzoylhydrazone Phenylhydrazone (31400-24-5) + butane-2,3-dione-bis-phenylhydrazone (2861-48-5)

Guidance literature:

With acetic acid; In ethanol; water; for 0.0166667h; Yields of byproduct given; Heating;

DOI:10.1021/jo00034a013

Reference yield: 76.0%

Biacetyl Benzoylhydrazone Phenylhydrazone (31400-24-5) → N-Benzoyl-2-phenyl-4,5-dimethyl-1,2,3-triazol-1-imine (138815-29-9)

Guidance literature:

With lead(IV) acetate; In acetonitrile;

DOI:10.1021/jo00034a013

Reference yield:

Biacetyl Benzoylhydrazone Phenylhydrazone (31400-24-5) → benzamide (55-21-0,27208-38-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / Pb(OAc)4 / acetonitrile

2: 45 percent / DMSO / 10 h / Irradiation

With lead(IV) acetate; dimethyl sulfoxide; In acetonitrile;

DOI:10.1021/jo00034a013

upstream raw materials:

biacetyl monobenzoyl hydrazone

phenylhydrazine

Downstream raw materials:

N-Benzoyl-2-phenyl-4,5-dimethyl-1,2,3-triazol-1-imine

4,5-Dimethyl-2-phenyl-2H-1,2,3-triazole

N-(benzoyl)-S,S-dimethylsulfoximine

N,N'-methylenebisbenzamide

Refernces