Technology Process of azo-1-cyclopropylcyclhexane
There total 4 articles about azo-1-cyclopropylcyclhexane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; iodine pentafluoride;
In
dichloromethane;
at -20 - 0 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 91 percent / NaN3, CF3COOH / CHCl3 / 4 h
2: LAH / diethyl ether / 1.) 12 h, 2.) reflux, 1 h
3: 11 percent / IF5, pyridine / CH2Cl2 / 2 h / -20 - 0 °C
With
pyridine; lithium aluminium tetrahydride; sodium azide; iodine pentafluoride; trifluoroacetic acid;
In
diethyl ether; dichloromethane; chloroform;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) t-BuLi / 1.) ether, pentane, -78 deg C, 1 h, 2.) a) -78 deg C, 4 h, b) from -78 deg C to RT, 3 h
2: 91 percent / NaN3, CF3COOH / CHCl3 / 4 h
3: LAH / diethyl ether / 1.) 12 h, 2.) reflux, 1 h
4: 11 percent / IF5, pyridine / CH2Cl2 / 2 h / -20 - 0 °C
With
pyridine; lithium aluminium tetrahydride; sodium azide; tert.-butyl lithium; iodine pentafluoride; trifluoroacetic acid;
In
diethyl ether; dichloromethane; chloroform;
