Trichloro(dichloromethyl)silane

Base Information Edit

Chemical Name:Trichloro(dichloromethyl)silane
CAS No.:1558-24-3
Molecular Formula:CHCl5Si
Molecular Weight:218.369
Hs Code.:
European Community (EC) Number:216-315-3
NSC Number:139833
DSSTox Substance ID:DTXSID7061778
Nikkaji Number:J206.784F
Wikidata:Q72510243
Mol file:1558-24-3.mol

Synonyms:Trichloro(dichloromethyl)silane;1558-24-3;(Dichloromethyl)trichlorosilane;Silane, trichloro(dichloromethyl)-;Dichloromethyltrichlorosilane;EINECS 216-315-3;NSC 139833;(Trichlorosilyl)dichloromethane;Dichloromethyl trichloro silane;CHCl5Si;C-H-Cl5-Si;SCHEMBL467765;DTXSID7061778;[Si](Cl)(Cl)(Cl)C(Cl)Cl;MFCD00045246;NSC139833;Trichloro(dichloromethyl)silane, 96%;AKOS008901232;NSC-139833;FT-0633663;J-009233

Suppliers and Price of Trichloro(dichloromethyl)silane

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
Trichloro(dichloromethyl)silane 96%
25ml
$ 326.00

American Custom Chemicals Corporation
(DICHLOROMETHYL)TRICHLOROSILANE 95.00%
25ML
$ 1284.94

AHH
(Dichloromethyl)trichlorosilane 98%
10g
$ 462.00

Total 36 raw suppliers

Chemical Property of Trichloro(dichloromethyl)silane Edit

Chemical Property:

Appearance/Colour:colorless clear liquid
Vapor Pressure:6.25mmHg at 25°C
Refractive Index:n20/D 1.474(lit.)
Boiling Point:145 °C at 760 mmHg
Flash Point:79.9 °C
PSA：0.00000
Density:1.552 g/cm³
LogP:3.40450
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:217.826065
Heavy Atom Count:7
Complexity:53.6

Purity/Quality:

97% ^*data from raw suppliers

Trichloro(dichloromethyl)silane 96% ^*data from reagent suppliers

Safty Information:

Pictogram(s): C
Hazard Codes:C
Statements: 10-14-34
Safety Statements: 16-23-26-36/37/39-45

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C([Si](Cl)(Cl)Cl)(Cl)Cl
Uses Trichloro(dichloromethyl)silane is a useful reagent for organic synthesis. It is used in the synthesis of silylated ethenes, acetylenes and other organosilicon compounds.

Technology Process of Trichloro(dichloromethyl)silane

There total 12 articles about Trichloro(dichloromethyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.5%

: 17760-13-3
trichloromethyltrichlorosilane

: 776-76-1
methyldiphenylsilane

: 1558-25-4
(chloromethyl)trichlorosilane

: 1558-24-3
trichloro(dichloromethyl)silane

: 144-79-6
chloromethyldiphenylsilane

Guidance literature:: at 160 - 240 ℃; for 6h;

Reference yield: 85.9%

: 75-79-6
Methyltrichlorosilane

: 1558-25-4
(chloromethyl)trichlorosilane

: 1558-24-3
trichloro(dichloromethyl)silane

: 17760-13-3
trichloromethyltrichlorosilane

Guidance literature:: With chlorine; at 250 ℃; for 20h; Further Variations:; Temperatures; time; Product distribution;
DOI:10.1023/A:1012753203518

Reference yield: 25.8%

: 67-66-3,8013-54-5
chloroform

: 10025-78-2
trichlorosilane

: 1,1,2,2-tetrachlorodisilane

: 10026-04-7,53609-55-5
tetrachlorosilane

: 31411-98-0
1,1,1,2,2-pentachlorodisilane

: 1558-24-3
trichloro(dichloromethyl)silane

: 13465-77-5
hexachlorodisilane

Guidance literature:: copyrolysis (1% CHCl3), quartz tube (575°C, retention time 30 s, yields of products depending on temperature (350 to 600°C)), product condensing; products not isolated, reaction monitoring by mass spectroscopy;
DOI:10.1007/BF02494755