N-butyl-2-ethylphenylamine

Base Information

• Chemical Name: N-butyl-2-ethylphenylamine
• CAS No.: 204926-79-4
• Molecular Formula: C₁₂H₁₉N
• Molecular Weight: 177.29
• Mol file: 204926-79-4.mol

Synonyms:N-butyl-2-ethylphenylamine

Chemical Property of N-butyl-2-ethylphenylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-butyl-2-ethylphenylamine

There total 5 articles about N-butyl-2-ethylphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

n-butyllithium (109-72-8,29786-93-4) + 1-azido-2-ethylbenzene (35774-47-1) → ortho-ethylaniline (578-54-1) + N-butyl-2-ethylphenylamine (204926-79-4)

Guidance literature:

In tetrahydrofuran; at -78 - 20 ℃; for 3h;

DOI:10.1002/jhet.275

Reference yield: 7.0%

C12H17N → N-butyl-2-ethylphenylamine (204926-79-4) + o-ethyl-N,N-dibutylaniline

Guidance literature:

With platinum-nickel nanoclusters on activated carbon; hydrogen; at 180 ℃; Flow reactor;

DOI:10.1134/S1070363218100018

Reference yield:

aniline (62-53-3) + butan-1-ol (71-36-3) → N-butyl-2-ethylphenylamine (204926-79-4) + 3-ethyl-2-propylquinoline (3290-24-2)

Guidance literature:

butan-1-ol; With iron chromite; dihydrogen peroxide; In water; at 20 ℃; for 2h; UV-irradiation;

aniline; In water; for 0.0833333h;

DOI:10.1134/S1070428018080080

upstream raw materials:

n-butyllithium

1-azido-2-ethylbenzene

1-bromo-butane

ortho-ethylaniline

Refernces

• 1、 Popov, Yu. V.,Mokhov,Latyshova,Nebykov,Panov,Davydova. "Colloidal and Nanosized Catalysts in Organic Synthesis: XX. Continuous Hydrogenation of Imines and Enamines Catalyzed by Nickel Nanoparticles". . p. 2035 - 2038. Retrieved 2018/12/11.
• 2、 Kim, Taehoon,Kim, Kyongtae. "N-butyllithium-mediated reactions of 1-(2-azidoarylmethyl)-1H- benzotriazoles with alkyl halides". experimental part. p. 98 - 111. Retrieved 2010/04/23.