4,4'-Bis(chloromethyl)-1,1'-biphenyl

Base Information Edit

Chemical Name:4,4'-Bis(chloromethyl)-1,1'-biphenyl
CAS No.:1667-10-3
Molecular Formula:C14H12Cl2
Molecular Weight:251.155
Hs Code.:29039990
European Community (EC) Number:216-784-4
NSC Number:74077
UNII:HZ7997EJT2
DSSTox Substance ID:DTXSID20168156
Nikkaji Number:J53.456K
Wikidata:Q72444658
Mol file:1667-10-3.mol

Synonyms:4,4'-Bis(chloromethyl)-1,1'-biphenyl;1667-10-3;4,4'-Bis(chloromethyl)biphenyl;1,1'-Biphenyl, 4,4'-bis(chloromethyl)-;1-(chloromethyl)-4-[4-(chloromethyl)phenyl]benzene;4,4-Bis(chloromethyl)-1,1-biphenyl;C14H12Cl2;4,4/'-Bis(chloromethyl)-1,1/'-biphenyl;EINECS 216-784-4;NSC-74077;4,4'-bis-(Chloromethyl)diphenyl;NSC74077;VANADIUMCARBIDE;4,4'-bischloromethylbiphenyl;SCHEMBL187751;p,p'-Bis(chloromethyl)biphenyl;HZ7997EJT2;1, 4,4'-bis(chloromethyl)-;DTXSID20168156;4,4'-bis-(chloromethyl)-biphenyl;4,4'-bischloromethyl-1,1'biphenyl;MFCD00674019;NSC 74077;AKOS015850604;p,p'-Bitolyl, alpha,alpha'-dichloro-;4,4'-Bis(chloromethyl)-1,1-biphenyl;AC-10394;4,4\'-Bis(chloromethyl)-1,1\'-biphenyl;4,4`-Bis( chloromethyl )-1,1`-biphenyl;B2099;FT-0617014;4,4'-Bis(chloromethyl)-1,1'-biphenyl, 95%;E76047;A810759;W-107918

Suppliers and Price of 4,4'-Bis(chloromethyl)-1,1'-biphenyl

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4,4''-Bis(chloromethyl)-1,1''-biphenyl
100g
$ 155.00

TCI Chemical
4,4'-Bis(chloromethyl)biphenyl
25G
$ 21.00

TCI Chemical
4,4'-Bis(chloromethyl)biphenyl
500G
$ 156.00

SynQuest Laboratories
4,4'-Bis(chloromethyl)-1,1'-biphenyl
500 g
$ 285.00

SynQuest Laboratories
4,4'-Bis(chloromethyl)-1,1'-biphenyl
100 g
$ 157.00

SynQuest Laboratories
4,4'-Bis(chloromethyl)-1,1'-biphenyl
25 g
$ 135.00

Sigma-Aldrich
4,4′-Bis(chloromethyl)-1,1′-biphenyl 95%
250g
$ 65.40

Matrix Scientific
4,4'-Bis(chloromethyl)-1,1'-biphenyl 95+%
10g
$ 15.00

Matrix Scientific
4,4'-Bis(chloromethyl)-1,1'-biphenyl 95+%
100g
$ 49.00

Frontier Specialty Chemicals
4,4'-Bis(chloromethyl)-1,1'-biphenyl 98%
500g
$ 233.00

Total 131 raw suppliers

Chemical Property of 4,4'-Bis(chloromethyl)-1,1'-biphenyl Edit

Chemical Property:

Appearance/Colour:white to off-white powder
Vapor Pressure:4.6Pa at 20℃
Melting Point:126 °C (dec.)(lit.)
Boiling Point:380 °C at 760 mmHg
Flash Point:196.3 °C
PSA：0.00000
Density:1.195 g/cm³
LogP:4.83120
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C
Solubility.:soluble in Tetrahydrofuran
Water Solubility.:200ng/L at 20℃
XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:250.0316058
Heavy Atom Count:16
Complexity:167

Purity/Quality:

98% ^*data from raw suppliers

4,4''-Bis(chloromethyl)-1,1''-biphenyl ^*data from reagent suppliers

Safty Information:

Pictogram(s): C
Hazard Codes:C
Statements: 34
Safety Statements: 26-27-36/37/39-45

MSDS Files:: SDS file from LookChem

Useful:

Chemical Classes:Other Classes -> Halogenated Polyaromatics
Canonical SMILES:C1=CC(=CC=C1CCl)C2=CC=C(C=C2)CCl

Technology Process of 4,4'-Bis(chloromethyl)-1,1'-biphenyl

There total 10 articles about 4,4'-Bis(chloromethyl)-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.7%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 92-52-4,1594-86-1
biphenyl

: 1667-10-3
4,4'-bis(chloromethyl)biphenyl

Guidance literature:: With hydrogenchloride; chloroacetic acid; In cyclohexane; at 20 - 40 ℃; for 6.5h; Reagent/catalyst; Time; Molecular sieve; Sonication; Large scale;

Reference yield: 95.3%

: 613-33-2
(4,4'-dimethyl-1,1'-biphenyl)

: 1667-10-3
4,4'-bis(chloromethyl)biphenyl

Guidance literature:: (4,4'-dimethyl-1,1'-biphenyl); With sulfuryl dichloride; 2,2'-azobis(isobutyronitrile); 7,7',8,8'-tetracyanoquinodimethane; In chlorobenzene; at 62 - 67 ℃; for 1.08333h; Inert atmosphere;

With sulfuryl dichloride; 2,2'-azobis(isobutyronitrile); 7,7',8,8'-tetracyanoquinodimethane; In chlorobenzene; for 0.833333h; Temperature; Reagent/catalyst; Solvent; Inert atmosphere;