benzyl 3,4,5-trimethoxyphenethylcarbamate

Base Information

• Chemical Name: benzyl 3,4,5-trimethoxyphenethylcarbamate
• CAS No.: 1436392-06-1
• Molecular Formula: C₁₉H₂₃NO₅
• Molecular Weight: 345.395
• Mol file: 1436392-06-1.mol

Synonyms:benzyl 3,4,5-trimethoxyphenethylcarbamate

Chemical Property of benzyl 3,4,5-trimethoxyphenethylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of benzyl 3,4,5-trimethoxyphenethylcarbamate

There total 1 articles about benzyl 3,4,5-trimethoxyphenethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

3-(3,4,5-trimethoxyphenyl)propanoic acid (25173-72-2) + benzyl alcohol (100-51-6,185532-71-2) → benzyl 3,4,5-trimethoxyphenethylcarbamate (1436392-06-1)

Guidance literature:

3-(3,4,5-trimethoxyphenyl)propanoic acid; With diphenyl phosphoryl azide; triethylamine; In benzene;

benzyl alcohol; In benzene; at 80 ℃; for 30h;

DOI:10.1016/j.bmc.2013.03.077

Reference yield: 84.0%

benzyl 3,4,5-trimethoxyphenethylcarbamate (1436392-06-1) → mescaline hydrochloride (832-92-8)

Guidance literature:

benzyl 3,4,5-trimethoxyphenethylcarbamate; With palladium on activated charcoal; hydrogen; In methanol; chloroform; for 24h;

With hydrogenchloride; In methanol; diethyl ether; water;

DOI:10.1016/j.bmc.2013.03.077

Reference yield:

benzyl 3,4,5-trimethoxyphenethylcarbamate (1436392-06-1) → mescaline (54-04-6)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogen; palladium on activated charcoal / methanol; chloroform / 24 h

2: sodium hydroxide / methanol / 3 h / 20 °C

With palladium on activated charcoal; hydrogen; sodium hydroxide; In methanol; chloroform;

DOI:10.1016/j.bmc.2013.03.077

upstream raw materials:

3-(3,4,5-trimethoxyphenyl)propanoic acid

benzyl alcohol

Downstream raw materials:

mescaline hydrochloride

mescaline

tert-butyl N-(3,4,5-trimethoxyphenethyl)sulfamoylcarbamate

N-(3,4,5-trimethoxyphenethyl)sulfamide

Refernces