benzyl i-butyl sulphide

Base Information

• Chemical Name: benzyl i-butyl sulphide
• CAS No.: 22336-60-3
• Molecular Formula: C₁₁H₁₆S
• Molecular Weight: 180.314
• Mol file: 22336-60-3.mol

Synonyms:benzyl i-butyl sulphide

Chemical Property of benzyl i-butyl sulphide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl i-butyl sulphide

There total 3 articles about benzyl i-butyl sulphide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.4%

Isobutyl bromide (78-77-3) + benzyl bromide (100-39-0) → benzyl i-butyl sulphide (22336-60-3)

Guidance literature:

With potassium carbonate; thiourea; In N,N-dimethyl-formamide; at 100 ℃; for 8h; Green chemistry;

DOI:10.1080/10426507.2014.919295

Reference yield:

benzyl thiocyanate (3012-37-1) + isobutylmagnesium bromide (926-62-5) → benzyl i-butyl sulphide (22336-60-3) + phenylmethanethiol (100-53-8)

Guidance literature:

With diethyl ether;

DOI:10.1021/ja01456a033

Reference yield:

phenylmethanethiol (100-53-8) → benzyl i-butyl sulphide (22336-60-3)

Guidance literature:

With ethanol; sodium ethanolate;

DOI:10.1002/hlca.19520350514

upstream raw materials:

benzyl thiocyanate

isobutylmagnesium bromide

phenylmethanethiol

Isobutyl bromide

Downstream raw materials:

(α-Benzoyloxy-benzyl)-isobutyl-sulfid

benzyl isobutyl sulfoxide

Refernces