<β-(tert-butyldioxy)phenethyl>chloromercury

Base Information

• Chemical Name: <β-(tert-butyldioxy)phenethyl>chloromercury
• CAS No.: 28531-39-7
• Molecular Formula: C₁₂H₁₇ClHgO₂
• Molecular Weight: 429.309
• Mol file: 28531-39-7.mol

Synonyms:<β-(tert-butyldioxy)phenethyl>chloromercury

Chemical Property of <β-(tert-butyldioxy)phenethyl>chloromercury

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of <β-(tert-butyldioxy)phenethyl>chloromercury

There total 1 articles about <β-(tert-butyldioxy)phenethyl>chloromercury which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ <β-(tert-butyldioxy)phenethyl>chloromercury (28531-39-7)

Guidance literature:

Styrol 1) tert-Butylhydroperoxid, Quecksilber(II)-acetat 2) NaCl(waess. Lsg.);

Reference yield: 84.0%

<β-(tert-butyldioxy)phenethyl>chloromercury (28531-39-7) → 1-Phenylethanol (98-85-1,13323-81-4) + (2-oxo-2-phenylethyl)mercury chloride (28531-58-0) + 1,1'-(1,2-ethanediyl)bisbenzene (103-29-7) + acetophenone (98-86-2) + acetone (67-64-1) + tert-butyl alcohol (75-65-0)

Guidance literature:

In toluene; at 90 - 140 ℃; Kinetics; Rate constant; nonane as solvent was used as well. Influence of azobisisobutyronitrile and ionol was tested;

Reference yield:

<β-(tert-butyldioxy)phenethyl>chloromercury (28531-39-7) → α-phenyl-β-chloromercuroethanol (39849-96-2) + (2-oxo-2-phenylethyl)mercury chloride (28531-58-0) + mercury(I) chloride (104923-33-3)

Guidance literature:

In toluene; byproducts: (CH3)3COH, (C6H5CH2)2, (C6H5)CH(OH)CH3; 140°C; further org. products; ppt. filtration off, washing (dry solvent); chem. and chromatographic anal. of ppt. and filtrate;

Downstream raw materials:

1-Phenylethanol

(2-oxo-2-phenylethyl)mercury chloride

1,1'-(1,2-ethanediyl)bisbenzene

acetophenone