2,4-dihydroxyl-6-pentylbenzaldehyde

Base Information Edit

Chemical Name:2,4-dihydroxyl-6-pentylbenzaldehyde
CAS No.:855875-40-0
Molecular Formula:C₁₂H₁₆O₃
Molecular Weight:208.257
Hs Code.:
Mol file:855875-40-0.mol

Synonyms:2,4-dihydroxyl-6-pentylbenzaldehyde

Suppliers and Price of 2,4-dihydroxyl-6-pentylbenzaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 2,4-dihydroxyl-6-pentylbenzaldehyde Edit

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 2,4-dihydroxyl-6-pentylbenzaldehyde

There total 8 articles about 2,4-dihydroxyl-6-pentylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 500-66-3
Olivetol

: 855875-40-0
2,4-dihydroxyl-6-pentylbenzaldehyde

Guidance literature:: With trichlorophosphate; at 0 - 20 ℃; for 8.5h; regioselective reaction; Inert atmosphere;
DOI:10.1021/acs.jnatprod.8b00227

Reference yield:

: 2,4-dimethoxy-6-pentyl-benzaldehyde

: 855875-40-0
2,4-dihydroxyl-6-pentylbenzaldehyde

Guidance literature:: With aluminum (III) chloride; In dichloromethane; at 20 - 40 ℃;

Reference yield:

: 20469-65-2
1-bromo-3,5-dimethoxybenzene

: 855875-40-0
2,4-dihydroxyl-6-pentylbenzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: magnesium / tetrahydrofuran / 30 - 40 °C

1.2: 35 °C / Reflux

2.1: N-Bromosuccinimide / dichloromethane / 0.5 h / 10 - 20 °C

3.1: magnesium / tetrahydrofuran / 30 - 40 °C

3.2: 1 h / 35 °C / Reflux

4.1: aluminum (III) chloride / dichloromethane / 20 - 40 °C

With aluminum (III) chloride; N-Bromosuccinimide; magnesium; In tetrahydrofuran; dichloromethane;