N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

Base Information Edit

Chemical Name:N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester
CAS No.:100945-15-1
Molecular Formula:C₁₃H₁₈NO₇P
Molecular Weight:331.262
Hs Code.:
Mol file:100945-15-1.mol

Synonyms:N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

Suppliers and Price of N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 3 raw suppliers

Chemical Property of N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester Edit

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

There total 8 articles about N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 127357-37-3,58237-86-8
methyl 2-(benzyloxycarbonylamino)-2-methoxyacetate

: 121-45-9
phosphorous acid trimethyl ester

: 100945-15-1,88568-95-0
N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

Guidance literature:: methyl 2-(benzyloxycarbonylamino)-2-methoxyacetate; With phosphorus trichloride; In toluene; at 70 ℃; for 12h;

phosphorous acid trimethyl ester; In toluene; at 70 ℃; for 4h;

Reference yield:

: 621-84-1
O-benzyl carbamate

: 100945-15-1,88568-95-0
N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.2: H⁺

2.1: 85 percent / PCl₃

With phosphorus trichloride;
DOI:10.1021/jo0106593

Reference yield:

: 121-45-9
phosphorous acid trimethyl ester

: methyl N-benzyloxycarbonyl-α-triphenylphosphonioglycinate tetrafluoroborate

: C₁₉H₁₈P⁽¹⁺⁾*C₁₂H₁₅NO₇P^(1-)

: 100945-15-1,88568-95-0
N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

Guidance literature:: phosphorous acid trimethyl ester; methyl N-benzyloxycarbonyl-α-triphenylphosphonioglycinate tetrafluoroborate; With methyl-triphenylphosphonium iodide; In dichloromethane; at 20 - 45 ℃;

With methyl iodide; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/j.tetlet.2006.03.051