hydrazinium mesylate

Base Information

• Chemical Name: hydrazinium mesylate
• CAS No.: 76391-43-0
• Molecular Formula: CH₄O₃S*H₄N₂
• Molecular Weight: 128.152
• Mol file: 76391-43-0.mol

Synonyms:hydrazinium mesylate

Chemical Property of hydrazinium mesylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of hydrazinium mesylate

There total 2 articles about hydrazinium mesylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

methyl fluorosulfonate (558-25-8) → trimethylsilyl fluoride (420-56-4) + Hexamethyldisiloxane (107-46-0) + Ammonium methanesulfonate (22515-76-0) + hydrazinium mesylate (76391-43-0)

Guidance literature:

With O-Trimethylsilylhydroxylamine;

Reference yield:

→ hydrazinium mesylate (76391-43-0) + fluconazole (86386-73-4)

Guidance literature:

Reference yield: 98.0%

hydrazinium mesylate (76391-43-0) + 2',4'-difluoropropiophenone (85068-30-0) → 1-cyclohexyl-3-ethyl-6-fluoro-1H-indazole (224048-17-3)

Guidance literature:

With sodium acetate; In toluene;

upstream raw materials:

methyl fluorosulfonate

Downstream raw materials:

1-cyclohexyl-3-ethyl-6-fluoro-1H-indazole

Refernces

• 1、 Brink, Klaus,Bliefert, Claus. "Mesylhydroxylamines, III. The Reaction of Methane Sulfonyl Fluoride and Hydroxyamine". . p. 1059 - 1062. Retrieved 2007/10/02.