Au(C₆F₅)C₂H^(1-)*((C₆H₅)3P)2N⁽¹⁺⁾=Au(C₆F₅)C₂H(((C₆H₅)3P)2N)

Base Information

• Chemical Name: Au(C₆F₅)C₂H^(1-)*((C₆H₅)3P)2N⁽¹⁺⁾=Au(C₆F₅)C₂H(((C₆H₅)3P)2N)
• CAS No.: 277303-32-9
• Molecular Formula: C₈HAuF₅*C₃₆H₃₀NP₂
• Molecular Weight: 927.643
• Mol file: 277303-32-9.mol

Synonyms:Au(C₆F₅)C₂H^(1-)*((C₆H₅)3P)2N⁽¹⁺⁾=Au(C₆F₅)C₂H(((C₆H₅)3P)2N)

Chemical Property of Au(C₆F₅)C₂H^(1-)*((C₆H₅)3P)2N⁽¹⁺⁾=Au(C₆F₅)C₂H(((C₆H₅)3P)2N)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Au(C₆F₅)C₂H^(1-)*((C₆H₅)3P)2N⁽¹⁺⁾=Au(C₆F₅)C₂H(((C₆H₅)3P)2N)

There total 1 articles about Au(C₆F₅)C₂H^(1-)*((C₆H₅)3P)2N⁽¹⁺⁾=Au(C₆F₅)C₂H(((C₆H₅)3P)2N) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

bis(triphenylphosphane)iminium(pentafluorophenyl)chlorogold(I) (74558-90-0) + acetylene (74-86-2,25067-58-7) → Au(C6F5)C2H(1-)*((C6H5)3P)2N(1+)=Au(C6F5)C2H(((C6H5)3P)2N) (277303-32-9)

Guidance literature:

With thallium acetylacetonate; In dichloromethane; byproducts: TlCl; a soln. of Tl(acac) and Au-complex was stirred for 40 min, filtd. through Celite, C2H2 was bubbled through soln. for 30 min; filtd. through anhyd. MgSO4, concd., Et2O added, ppt. collected; elem. anal.;

DOI:10.1021/om9910322

Reference yield:

bis(triphenylphosphane)iminium(pentafluorophenyl)chlorogold(I) (74558-90-0) + Au(C6F5)C2H(1-)*((C6H5)3P)2N(1+)=Au(C6F5)C2H(((C6H5)3P)2N) (277303-32-9) → (Au(C6F5))2C2(2-)*2((C6H5)3P)2N(1+)=(Au(C6F5))2C2(((C6H5)3P)2N)2

Guidance literature:

With KOH; In acetone; byproducts: KCl; 48 h; evapd., extd. with CH2Cl2, filtd., filtrate concd., pentane added, ppt.collected; elem. anal.;

DOI:10.1021/om9910322

upstream raw materials:

bis(triphenylphosphane)iminium(pentafluorophenyl)chlorogold(I)

acetylene

Refernces