Technology Process of C23H23N3O2
There total 7 articles about C23H23N3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; dichloromethane;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrahydrofuran / 0 - 5 °C / Inert atmosphere
2.1: hydrogenchloride / water / 1 h / 20 °C
2.2: pH 9 - 10 / Cooling with ice
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane; tetrahydrofuran / 20 °C
With
hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: hydrogenchloride / water / 1 h / 20 °C
1.2: pH 9 - 10 / Cooling with ice
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane; tetrahydrofuran / 20 °C
With
hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; dichloromethane; water;