Technology Process of 2-(t-butoxycarbonylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether
There total 9 articles about 2-(t-butoxycarbonylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanol; sodium tetrahydroborate;
at 0 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dichloromethane / 20 °C / Inert atmosphere
2: sodium hydroxide / tetra-(n-butyl)ammonium iodide / dichloromethane; water / Inert atmosphere
3: hydrogen; ammonia / palladium on activated charcoal / tetrahydrofuran; methanol / 1 h / 760.05 Torr
4: methanol
5: sodium tetrahydroborate; methanol / 2 h / 0 °C
With
methanol; sodium tetrahydroborate; ammonia; hydrogen; sodium hydroxide;
palladium on activated charcoal; tetra-(n-butyl)ammonium iodide;
In
tetrahydrofuran; methanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydroxide / tetra-(n-butyl)ammonium iodide / dichloromethane; water / Inert atmosphere
2: hydrogen; ammonia / palladium on activated charcoal / tetrahydrofuran; methanol / 1 h / 760.05 Torr
3: methanol
4: sodium tetrahydroborate; methanol / 2 h / 0 °C
With
methanol; sodium tetrahydroborate; ammonia; hydrogen; sodium hydroxide;
palladium on activated charcoal; tetra-(n-butyl)ammonium iodide;
In
tetrahydrofuran; methanol; dichloromethane; water;
