Technology Process of C16H16FN5O
There total 8 articles about C16H16FN5O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C16H19FN4O5S;
With
hydrogenchloride;
In
water;
at 20 ℃;
With
sodium hydroxide;
In
water;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: sodium methylate / methanol / 3 h / 70 °C
1.2: 1 h / 0 - 20 °C
2.1: water; acetone / 3 h / 0 - 20 °C
3.1: hydroxylamine hydrochloride; sodium acetate / methanol / 0.5 h / Heating / reflux
4.1: triethylamine / dichloromethane / 20 °C
5.1: tetrahydrofuran / 0 - 20 °C
5.2: 4 h / 0 - 20 °C
6.1: diethyl ether / 0.5 h / 0 - 20 °C
7.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 2 h / 0 - 20 °C
8.1: hydrogenchloride / water / 20 °C
With
hydrogenchloride; hydroxylamine hydrochloride; sodium methylate; sodium acetate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; water; acetone;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydroxylamine hydrochloride; sodium acetate / methanol / 0.5 h / Heating / reflux
2.1: triethylamine / dichloromethane / 20 °C
3.1: tetrahydrofuran / 0 - 20 °C
3.2: 4 h / 0 - 20 °C
4.1: diethyl ether / 0.5 h / 0 - 20 °C
5.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 2 h / 0 - 20 °C
6.1: hydrogenchloride / water / 20 °C
With
hydrogenchloride; hydroxylamine hydrochloride; sodium acetate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; water;