C₄₆H₄₁N₁₁O₄

Base Information Edit

Chemical Name:C₄₆H₄₁N₁₁O₄
CAS No.:1612874-02-8
Molecular Formula:C₄₆H₄₁N₁₁O₄
Molecular Weight:811.903
Hs Code.:
Mol file:1612874-02-8.mol

C<sub>46</sub>H<sub>41</sub>N<sub>11</sub>O<sub>4</sub>

Synonyms:C₄₆H₄₁N₁₁O₄

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Chemical Property of C₄₆H₄₁N₁₁O₄ Edit

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Technology Process of C₄₆H₄₁N₁₁O₄

There total 9 articles about C₄₆H₄₁N₁₁O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 36171-39-8
1-pyrenyl azide

: 1612874-01-7
C₃₀H₃₂N₈O₄

: 1612874-02-8
C₄₆H₄₁N₁₁O₄

Guidance literature:: With copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 20 ℃; for 5h;
DOI:10.1002/ejoc.201301838

Reference yield:

: 6310-19-6
4-tert-butyl-2-nitroaniline

: 1612874-02-8
C₄₆H₄₁N₁₁O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: Iodine monochloride / 1,2-dichloro-ethane / 3 h / 70 °C / Inert atmosphere

2.1: sodium nitrite; sulfuric acid / ethanol / 0 °C / Reflux

3.1: tin(II) chloride dihdyrate; ethanol / Reflux

4.1: sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(l) iodide; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 1 h / 20 °C

5.1: sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(II) sulfate / water; tetrahydrofuran / 12 h / 20 °C

6.1: dicyclohexyl-carbodiimide / dichloromethane / 0.17 h

6.2: 0.5 h

7.1: copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 5 h / 20 °C

With copper(l) iodide; sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; tin(II) chloride dihdyrate; ethanol; sulfuric acid; Iodine monochloride; copper(II) sulfate; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; N,N`-dimethylethylenediamine; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide; 1,2-dichloro-ethane; toluene;
DOI:10.1002/ejoc.201301838

Reference yield:

: 1369827-82-6
C₁₀H₁₂INO₂

: 1612874-02-8
C₄₆H₄₁N₁₁O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: tin(II) chloride dihdyrate; ethanol / Reflux

2.1: sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(l) iodide; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 1 h / 20 °C

3.1: sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(II) sulfate / water; tetrahydrofuran / 12 h / 20 °C

4.1: dicyclohexyl-carbodiimide / dichloromethane / 0.17 h

4.2: 0.5 h

5.1: copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 5 h / 20 °C

With copper(l) iodide; sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; tin(II) chloride dihdyrate; ethanol; copper(II) sulfate; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; N,N`-dimethylethylenediamine; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; toluene;
DOI:10.1002/ejoc.201301838