2-IODO-3-NITRONAPHTHALENE

Base Information

• Chemical Name: 2-IODO-3-NITRONAPHTHALENE
• CAS No.: 102153-71-9
• Molecular Formula: C10H6INO2
• Molecular Weight: 299.068
• Hs Code.: 2904909090
• Mol file: 102153-71-9.mol

Synonyms:2-IODO-3-NITRONAPHTHALENE

Chemical Property of 2-IODO-3-NITRONAPHTHALENE

Chemical Property:

• Vapor Pressure: 6.38E-06mmHg at 25°C
• Refractive Index: 1.74
• Boiling Point: 389.5 °C at 760 mmHg
• Flash Point: 189.3 °C
• PSA: 45.82000
• Density: 1.899 g/cm³
• LogP: 3.87580

Purity/Quality:

98%Min ^*data from raw suppliers

2-Iodo-3-nitronaphthalene ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-IODO-3-NITRONAPHTHALENE

There total 8 articles about 2-IODO-3-NITRONAPHTHALENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2-bromo-3-nitronaphthalene (67116-33-0) → 2-iodo-3-nitronaphthalene (102153-71-9)

Guidance literature:

With copper(l) iodide; potassium iodide; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 150 ℃; for 3h;

DOI:10.1016/S0040-4039(00)00263-X

Reference yield: 70.9%

2-nitronaphthalene (581-89-5) → 2-iodo-3-nitronaphthalene (102153-71-9)

Guidance literature:

With potassium iodate; sulfuric acid; iodine; acetic acid; In water; at 40 ℃; for 5h;

Reference yield:

→ 2-iodo-3-nitronaphthalene (102153-71-9)

Guidance literature:

With bromine; at 130 - 160 ℃;

DOI:10.1039/jr9310003176

upstream raw materials:

3-nitronaphthalen-2-amine

3-iodo-2-nitro-[1]naphthylamine

2-bromo-3-nitronaphthalene

N-(3-iodo-2-nitro-[1]naphthyl)-acetamide

Downstream raw materials:

2-amino-3-iodonaphthalene

2-nitronaphthalene

dinaphtho[2,3-b:2′,3′-d]furan

Dibenzo[b,h]biphenylene

Refernces

• 1、 Hodgson,Hathway. "-". . p. 123,125. Retrieved 1945.
• 2、 -. "Fluorene-containing organic compound as well as preparation method and application thereof in OLED (organic light emitting diode) device". Paragraph 0103-0105. . Retrieved 2018/04/21.