4-(DIMETHYLAMINO) CYCLOHEXANOL

Base Information

• Chemical Name: 4-(DIMETHYLAMINO) CYCLOHEXANOL
• CAS No.: 61168-09-0
• Molecular Formula: C₈H₁₇NO
• Molecular Weight: 143.229
• Hs Code.: 2922199090
• Mol file: 61168-09-0.mol

Synonyms:4-Dimethylaminocyclohexanol;4-Hydroxy-N,N-dimethylcyclohexylamine;

Chemical Property of 4-(DIMETHYLAMINO) CYCLOHEXANOL

Chemical Property:

• Boiling Point: 216.4 °C at 760 mmHg
• Flash Point: 86.1 °C
• PSA: 23.47000
• Density: 0.97 g/cm³
• LogP: 0.85150
• Storage Temp.: 2-8°C

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-(Dimethylamino)cyclohexanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(DIMETHYLAMINO) CYCLOHEXANOL

There total 6 articles about 4-(DIMETHYLAMINO) CYCLOHEXANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ N,N-dimethyl-cyclohexanamine (98-94-2) + 4-(dimethylamino)cyclohexanol (103023-50-3,103023-51-4,61168-09-0)

Guidance literature:

With water; platinum; under 2280 Torr; Hydrogenation_.entsteht ein Gemisch der diastereoisomeren Formen;

Reference yield:

4-(N,N-dimethylamino)phenol (619-60-3) + water (7732-18-5) → N,N-dimethyl-cyclohexanamine (98-94-2) + 4-(dimethylamino)cyclohexanol (103023-50-3,103023-51-4,61168-09-0)

Guidance literature:

under 2280 Torr; Reaktion des Hydrochlorids_.Hydrogenation;

Reference yield:

trans-N-acetyl-4-hydroxycyclohexylamine (23363-88-4) → 4-(dimethylamino)cyclohexanol (103023-50-3,103023-51-4,61168-09-0)

Guidance literature:

With potassium hydroxide; Hydrolysis_.anschliessenden Reaktion mit Formaldehyd und Ameisensaeure;

DOI:10.1021/jo01361a003

upstream raw materials:

trans-N-acetyl-4-hydroxycyclohexylamine

formaldehyd

4-(N,N-dimethylamino)phenol

water

Downstream raw materials:

N,N,N-trimethyl-4-(thiophen-3-ylmethylene)cyclohexanaminium bromide

4-(dimethylamino)cyclohexanone

Refernces

• 1、 Denmark, Scott E.,Forbes, David C.,Hays, David S.,DePue, Jeffrey S.,Wilde, Richard G.. "Catalytic Epoxidation of Alkenes with Oxone". . p. 1391 - 1407. Retrieved 2007/10/02.