C₁₃H₁₅NO₄

Base Information

• Chemical Name: C₁₃H₁₅NO₄
• CAS No.: 1403957-00-5
• Molecular Formula: C₁₃H₁₅NO₄
• Molecular Weight: 249.266
• Mol file: 1403957-00-5.mol

Synonyms:C₁₃H₁₅NO₄

Chemical Property of C₁₃H₁₅NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₃H₁₅NO₄

There total 1 articles about C₁₃H₁₅NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

para-acetylphenylalanine (18910-27-5,22888-49-9,122555-04-8) + acetic acid (64-19-7,77671-22-8) → C13H15NO4 (1403957-00-5)

Guidance literature:

With acetic anhydride; at 20 ℃; for 2h;

Reference yield:

C13H15NO4 (1403957-00-5) → para-acetyl-phenylalanine (204716-07-4,1217751-18-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: Acylase I; cobalt(II) chloride hexahydrate / aq. phosphate buffer / 24 h / 37 °C / Enzymatic reaction

1.2: 0.08 h / 60 °C / pH 8

2.1: sodium hydrogencarbonate / water; acetone / 3 h

With Acylase I; cobalt(II) chloride hexahydrate; sodium hydrogencarbonate; In aq. phosphate buffer; water; acetone;

Reference yield:

C13H15NO4 (1403957-00-5) → p-acetyl-L-phenylalanine (122555-04-8) + C13H15NO4

Guidance literature:

C₁₃H₁₅NO₄; With Acylase I; cobalt(II) chloride hexahydrate; In aq. phosphate buffer; at 37 ℃; for 24h; Enzymatic reaction;

With lithium hydroxide; at 60 ℃; for 0.0833333h; pH=8;

upstream raw materials:

para-acetylphenylalanine

acetic acid

Downstream raw materials:

p-acetyl-L-phenylalanine

para-acetyl-phenylalanine

Refernces