1,1,1,3-TETRACHLORODECANE

Base Information

• Chemical Name: 1,1,1,3-TETRACHLORODECANE
• CAS No.: 51755-60-3
• Molecular Formula: C₁₀H₁₈Cl₄
• Molecular Weight: 280.065
• Hs Code.: 2903199000
• Mol file: 51755-60-3.mol

Synonyms:1,1,1,3-TETRACHLORODECANE

Chemical Property of 1,1,1,3-TETRACHLORODECANE

Chemical Property:

• Boiling Point: 298.0±8.0 °C(Predicted)
• PSA: 0.00000
• Density: 1.169±0.06 g/cm3(Predicted)
• LogP: 5.71460

Purity/Quality:

98% ^*data from raw suppliers

1,1,1,3-Tetrachlorodecane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 1,1,1,3-Tetrachlorodecane is used in the synthesis of bis(2-pyridylmethyl)amine copper complexes, which exhibits catalytic activity.Also, it is derived from Carbon Tetrachloride (C176905), which is used in biological studies to evaluate the genotoxicity and toxicity in primary hepatocyte culture of humans and lab animals.Persistent environmental pollutant.

Technology Process of 1,1,1,3-TETRACHLORODECANE

There total 4 articles about 1,1,1,3-TETRACHLORODECANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

Trichloromethanesulfonyl chloride (2547-61-7) + non-1-ene (124-11-8) → 1,1,1,3-tetrachlorodecane (51755-60-3)

Guidance literature:

dichlorotris(triphenylphosphine)ruthenium(II); In benzene; at 140 ℃; for 36h;

Reference yield:

1-Decene (872-05-9,17438-89-0,25189-70-2) → 1,1,1,3-tetrachlorodecane (51755-60-3)

Guidance literature:

With tetrachloromethane; 2,2'-azobis(isobutyronitrile); C₁₆H₁₉ClCuN₃⁽¹⁺⁾*ClO₄^(1-); In acetonitrile; at 60 ℃; for 24h; Reagent/catalyst; Catalytic behavior; Inert atmosphere; Sealed tube;

DOI:10.1016/j.poly.2015.12.043

Reference yield:

tetrachloromethane (56-23-5) + non-1-ene (124-11-8) → 1,1,1,3-tetrachlorodecane (51755-60-3)

Guidance literature:

tris(triphenylphosphine)ruthenium(II) chloride; at 80 ℃; for 4h;

DOI:10.1016/S0040-4039(01)87410-4

upstream raw materials:

tetrachloromethane

non-1-ene

Trichloromethanesulfonyl chloride

1-Decene

Refernces

• 1、 Khusnutdinov,Shchadneva,Baiguzina,Lavrent'eva,Burangulova,Atnabaeva,Dzhemilev. "Addition of carbon tetrachloride to unsaturated compounds catalyzed by manganese, vanadium, and molybdenum complexes". . p. 350 - 357. Retrieved 2007/10/03.