27-hydroxy-octacosanoic acid methyl ester

Base Information

• Chemical Name: 27-hydroxy-octacosanoic acid methyl ester
• CAS No.: 775341-88-3
• Molecular Formula: C₂₉H₅₈O₃
• Molecular Weight: 454.778
• Mol file: 775341-88-3.mol

Synonyms:27-hydroxy-octacosanoic acid methyl ester

Chemical Property of 27-hydroxy-octacosanoic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 27-hydroxy-octacosanoic acid methyl ester

There total 2 articles about 27-hydroxy-octacosanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + lipopolysaccharide from Sinorhizobium fredii HH103, rkpA → 27-hydroxy-octacosanoic acid methyl ester (775341-88-3) + 3-hydroxy-octadecanoic acid methyl ester (2420-36-2) + β-hydroxyhexadecanoic acid methyl ester (51883-36-4) + methyl 3-hydroxytridecanoate (150024-70-7) + Methyl-3-hydroxypentadecanoat (112538-88-2) + β-hydroxydodecanoic acid methyl ester (72864-23-4,85464-97-7) + (+/-)-3-hydroxytetradecanoic acid methyl ester (55682-83-2) + Methyl 29-hydroxytriacontanoate + C18H36O3 (112538-92-8) + C20H40O3

Guidance literature:

With hydrogenchloride; In water; at 80 ℃; for 16h;

DOI:10.1074/jbc.ra120.013393

Reference yield:

methanol (67-56-1) + lipopolysaccharide from Sinorhizobium fredii HH103, rkpM → 27-hydroxy-octacosanoic acid methyl ester (775341-88-3) + 3-hydroxy-octadecanoic acid methyl ester (2420-36-2) + β-hydroxyhexadecanoic acid methyl ester (51883-36-4) + methyl 3-hydroxytridecanoate (150024-70-7) + Methyl-3-hydroxypentadecanoat (112538-88-2) + β-hydroxydodecanoic acid methyl ester (72864-23-4,85464-97-7) + (+/-)-3-hydroxytetradecanoic acid methyl ester (55682-83-2) + Methyl 29-hydroxytriacontanoate + C18H36O3 (112538-92-8) + C20H40O3

Guidance literature:

With hydrogenchloride; In water; at 80 ℃; for 16h;

DOI:10.1074/jbc.ra120.013393

Reference yield: 73.0%

27-hydroxy-octacosanoic acid methyl ester (775341-88-3) + benzaldehyde (100-52-7) → 27-benzyloxy-octacosanoic acid methyl ester (775341-74-7)

Guidance literature:

With triethylsilane; Hexamethyldisiloxane; trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; for 6h;

DOI:10.1021/ol048746f

upstream raw materials:

methanol

Downstream raw materials:

27-benzyloxy-octacosanoic acid methyl ester

27-benzyloxy-octacosanoic acid

Refernces