1,2,9,10-tetrathiacyclohexadecane

Base Information

• Chemical Name: 1,2,9,10-tetrathiacyclohexadecane
• CAS No.: 13375-94-5
• Molecular Formula: C₁₂H₂₄S₄
• Molecular Weight: 296.587
• Mol file: 13375-94-5.mol

Synonyms:1,2,9,10-tetrathiacyclohexadecane

Chemical Property of 1,2,9,10-tetrathiacyclohexadecane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1,2,9,10-tetrathiacyclohexadecane

There total 1 articles about 1,2,9,10-tetrathiacyclohexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

1,6-dimercaptohexane (1191-43-1) → 1,2-dithiacyclooctane (6008-69-1) + 1,2,9,10-tetrathiacyclohexadecane (13375-94-5)

Guidance literature:

With iodine; triethylamine; In chloroform; at 20 ℃; for 5h; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.inorgchem.7b01398

upstream raw materials:

1,6-dimercaptohexane

Refernces

• 1、 Kato, Eishin,Oya, Masayuki,Iso, Tadashi,Iwao, Jun-ichi. "Conversion of Thiols into Disulfides with Diethyl Bromomalonate". . p. 486 - 495. Retrieved 2007/10/02.