Technology Process of C36H48O7Si
There total 6 articles about C36H48O7Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-(tert-butyldiphenylsilyloxy)prop-1-ene;
With
9-bora-bicyclo[3.3.1]nonane;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
C18H23F3O9S;
With
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; potassium phosphate; triphenyl-arsane;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
at 45 ℃;
for 14.2h;
DOI:10.1002/anie.201104681
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium hexamethylsilazane / tetrahydrofuran / 1 h / -78 °C
1.2: 1.08 h / -78 - 20 °C
2.1: titanium(IV) tetraethanolate / ethanol / Heating
3.1: toluene-4-sulfonic acid / benzene / 17 h / Reflux
4.1: potassium hexamethylsilazane / tetrahydrofuran / -45 - -40 °C
4.2: 0.75 h / -40 - -30 °C
5.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 2 h / 20 °C
5.2: 14.2 h / 45 °C
With
titanium(IV) tetraethanolate; potassium hexamethylsilazane; toluene-4-sulfonic acid; 9-bora-bicyclo[3.3.1]nonane;
In
tetrahydrofuran; ethanol; benzene;
5.2: Suzuki cross-coupling;
DOI:10.1002/anie.201104681
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: titanium(IV) tetraethanolate / ethanol / Heating
2.1: toluene-4-sulfonic acid / benzene / 17 h / Reflux
3.1: potassium hexamethylsilazane / tetrahydrofuran / -45 - -40 °C
3.2: 0.75 h / -40 - -30 °C
4.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 2 h / 20 °C
4.2: 14.2 h / 45 °C
With
titanium(IV) tetraethanolate; potassium hexamethylsilazane; toluene-4-sulfonic acid; 9-bora-bicyclo[3.3.1]nonane;
In
tetrahydrofuran; ethanol; benzene;
4.2: Suzuki cross-coupling;
DOI:10.1002/anie.201104681
