9-BROMO-2-NITROFLUORENE

Base Information

• Chemical Name: 9-BROMO-2-NITROFLUORENE
• CAS No.: 53172-79-5
• Molecular Formula: C13H8 Br N O2
• Molecular Weight: 290.116
• Hs Code.: 2904909090
• Mol file: 53172-79-5.mol

Synonyms:Fluorene,9-bromo-2-nitro- (6CI,7CI); 2-Nitro-9-bromofluorene; 9-Bromo-2-nitrofluorene;NSC 12355

Chemical Property of 9-BROMO-2-NITROFLUORENE

Chemical Property:

• Vapor Pressure: 4.65E-06mmHg at 25°C
• Boiling Point: 394°C at 760 mmHg
• Flash Point: 192.1°C
• PSA: 45.82000
• Density: 1.662g/cm³
• LogP: 4.58270

Purity/Quality:

99%min ^*data from raw suppliers

9-BROMO-2-NITROFLUORENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 9-BROMO-2-NITROFLUORENE

There total 12 articles about 9-BROMO-2-NITROFLUORENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethanol (64-17-5) + dimethyl-(2-nitro-fluoren-9-yl)-sulfonium ; bromide (42729-97-5) → dimethylsulfide (75-18-3) + 9-bromo-2-nitro-fluorene (53172-79-5)

Guidance literature:

DOI:10.1039/jr9350001609

Reference yield:

2-nitro-9H-fluorene (607-57-8) → 9-bromo-2-nitro-fluorene (53172-79-5)

Guidance literature:

With tetrachloromethane; N-Bromosuccinimide;

Reference yield:

9H-fluoren-9-yl bromide (1940-57-4) → 9-bromo-2-nitro-fluorene (53172-79-5)

Guidance literature:

With nitric acid; acetic anhydride; at 0 ℃;

DOI:10.1039/jr9350001607

upstream raw materials:

tetrachloromethane

N-Bromosuccinimide

2-nitro-9H-fluorene

benzene

Downstream raw materials:

2-aminofluorene

9-bromo-2,7-dinitrofluorene

9-bromo-2,5-dinitro-fluorene

methyl-(2-nitro-fluoren-9-yl)-phenyl-amine