Technology Process of 1,1-diphenylpentylhydroperoxide
There total 11 articles about 1,1-diphenylpentylhydroperoxide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfuric acid; dihydrogen peroxide;
In
tetrahydrofuran; water;
at 0 - 60 ℃;
for 8h;
DOI:10.3762/bjoc.9.138
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 10 h / 0 - 60 °C
2.1: copper diacetate; 1,10-Phenanthroline; triethylamine; oxygen / toluene; acetonitrile / 20 °C
2.2: 20 °C
3.1: diethyl ether; hexane / -78 - 20 °C
4.1: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 8 h / 0 - 60 °C
With
1,10-Phenanthroline; sulfuric acid; dihydrogen peroxide; oxygen; copper diacetate; triethylamine;
In
tetrahydrofuran; diethyl ether; hexane; water; toluene; acetonitrile;
DOI:10.3762/bjoc.9.138
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 8 h / 0 - 60 °C
2.1: copper diacetate; 1,10-Phenanthroline; triethylamine; oxygen / toluene; acetonitrile / 20 °C
2.2: 20 °C
3.1: diethyl ether; hexane / -78 - 20 °C
4.1: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 8 h / 0 - 60 °C
With
1,10-Phenanthroline; sulfuric acid; dihydrogen peroxide; oxygen; copper diacetate; triethylamine;
In
tetrahydrofuran; diethyl ether; hexane; water; toluene; acetonitrile;
DOI:10.3762/bjoc.9.138