3,4,5-trichlorobenzenediazonium tetrafluoroborate

Base Information

• Chemical Name: 3,4,5-trichlorobenzenediazonium tetrafluoroborate
• CAS No.: 2106-38-9
• Molecular Formula: BF₄*C₆H₂Cl₃N₂
• Molecular Weight: 295.259
• Mol file: 2106-38-9.mol

Synonyms:3,4,5-trichlorobenzenediazonium tetrafluoroborate

Chemical Property of 3,4,5-trichlorobenzenediazonium tetrafluoroborate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,4,5-trichlorobenzenediazonium tetrafluoroborate

There total 1 articles about 3,4,5-trichlorobenzenediazonium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

3,4,5-trichloroaniline (634-91-3) → 3,4,5-trichlorobenzenediazonium tetrafluoroborate (2106-38-9)

Guidance literature:

With 2-Methyl-2-nitropropane; boron trifluoride diethyl etherate; In diethyl ether; dichloromethane; at -20 - 20 ℃; for 0.833333h;

Reference yield: 99.0%

3,4,5-trichlorobenzenediazonium tetrafluoroborate (2106-38-9) → 5-bromo-1,2,3-trichloro-benzene (21928-51-8)

Guidance literature:

With dibenzo-18-crown-6; potassium bromide; copper(ll) bromide; 1,10-Phenanthroline; copper(I) bromide; In acetonitrile; at 20 ℃; for 0.333333h;

DOI:10.1055/s-2007-983784

Reference yield: 49.0%

3,4,5-trichlorobenzenediazonium tetrafluoroborate (2106-38-9) → 3,4,5-trichlorophenol (609-19-8)

Guidance literature:

With copper(I) oxide; copper(II) nitrate; In water; at 20 ℃; for 1.16667h;

upstream raw materials:

3,4,5-trichloroaniline

Downstream raw materials:

5-bromo-1,2,3-trichloro-benzene

3,4,5-trichlorophenol

3,4,5-trichlorobenzenethiol

Refernces

• 1、 Korzeniowski, Stephen H.,Leopold, Ahuva,Beadle, James R.,Ahern, Michael F.,Sheppard, William A.,et al.. "Crown Cation Complex Effects. 12. Dissolution and Complexation of Arenediazonium Cations in Nonpolar Media. An Assessment of Solvent Effects and Reactivity by Infrared and Nuclear Magnetic Resonance Spectroscopy". . p. 2153 - 2159. Retrieved 2007/10/02.