Technology Process of 4-((3,3,4,4,5,5,6,6,6-nonafluorohexylthio)carbonyl)phenyl
There total 6 articles about 4-((3,3,4,4,5,5,6,6,6-nonafluorohexylthio)carbonyl)phenyl which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
acetonitrile;
at 20 ℃;
for 24h;
DOI:10.1021/ma101914j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C
2: ammonium hydroxide; water / ethanol; dichloromethane
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 24 h / 20 °C
With
ammonium hydroxide; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dicyclohexyl-carbodiimide;
In
ethanol; dichloromethane; acetonitrile;
DOI:10.1021/ma101914j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thallium(III) nitrate
2: water; sodium hydroxide
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 24 h / 20 °C
With
water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; thallium(III) nitrate; sodium hydroxide;
In
acetonitrile;
1: Willgerodt-Kindler reaction;
DOI:10.1021/ma101914j
