3,4-epoxy-3-phenylsulfinyl-nonanone

Base Information

• Chemical Name: 3,4-epoxy-3-phenylsulfinyl-nonanone
• CAS No.: 95110-50-2
• Molecular Formula: C₁₅H₂₂O₂S
• Molecular Weight: 266.404
• Mol file: 95110-50-2.mol

Synonyms:3,4-epoxy-3-phenylsulfinyl-nonanone

Chemical Property of 3,4-epoxy-3-phenylsulfinyl-nonanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,4-epoxy-3-phenylsulfinyl-nonanone

There total 6 articles about 3,4-epoxy-3-phenylsulfinyl-nonanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3-Benzenesulfinyl-3-chloro-nonan-4-ol (104354-48-5,104419-82-1) → 3,4-epoxy-3-phenylsulfinylnonane (95110-50-2,104420-51-1,104420-52-2)

Guidance literature:

With potassium hydroxide; In methanol; for 1h; Ambient temperature;

DOI:10.1246/bcsj.58.2849

Reference yield: 89.0%

3-Benzenesulfinyl-3-chloro-nonan-4-ol (104354-48-5,104419-82-1) → 3,4-epoxy-3-phenylsulfinylnonane (95110-50-2,104420-51-1,104420-52-2)

Guidance literature:

With potassium hydroxide; In methanol; for 1h; Ambient temperature;

DOI:10.1246/bcsj.58.2849

Reference yield:

[(1-chloropropyl)sulfinyl]benzene (104354-47-4) → 3,4-epoxy-3-phenylsulfinylnonane (95110-50-2,104420-51-1,104420-52-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) lithium diisopropyl amide / 1) THF, -60 deg C, 15 min, 2) THF, -60 deg C

2: 89 percent / 30percent aq. KOH / methanol / 1 h / Ambient temperature

With potassium hydroxide; lithium diisopropyl amide; In methanol;

DOI:10.1246/bcsj.58.2849

upstream raw materials:

3-Benzenesulfinyl-3-chloro-nonan-4-ol

3-Benzenesulfinyl-3-chloro-nonan-4-ol

[(1-chloropropyl)sulfinyl]benzene

hexanal

Downstream raw materials:

4-phenylthio-3-nonanone

Refernces