(CH₃)2(C₃HN₂Ge)(2,6-iPr₂C₆H₃)2OCHO

Base Information

• Chemical Name: (CH₃)2(C₃HN₂Ge)(2,6-iPr₂C₆H₃)2OCHO
• CAS No.: 1109286-34-1
• Molecular Formula: C₃₀H₄₂GeN₂O₂
• Molecular Weight: 535.266
• Mol file: 1109286-34-1.mol

Synonyms:(CH₃)2(C₃HN₂Ge)(2,6-iPr₂C₆H₃)2OCHO

Chemical Property of (CH₃)2(C₃HN₂Ge)(2,6-iPr₂C₆H₃)2OCHO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (CH₃)2(C₃HN₂Ge)(2,6-iPr₂C₆H₃)2OCHO

There total 1 articles about (CH₃)2(C₃HN₂Ge)(2,6-iPr₂C₆H₃)2OCHO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[C3H(CH3)2(N(2,6-diisopropylphenyl))2 chlorogermylene] (334719-93-6) → (CH3)2(C3HN2Ge)(2,6-iPr2C6H3)2OCHO (1109286-34-1)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran; toluene

2: toluene

In tetrahydrofuran; toluene;

Reference yield: 95.0%

(CH3)2(C3HN2Ge)(2,6-iPr2C6H3)2OCHO (1109286-34-1) → (HC(CMeNC-2,6-i-Pr2C6H3)2)-germanium(II) hydride (382150-90-5) + lithium formate (556-63-8)

Guidance literature:

With n-butyllithium; borane-ammonia complex; In tetrahydrofuran; hexane; at -78 - 20 ℃;

DOI:10.1039/c0dt00921k

Reference yield: 74.0%

[(HC(CMeN(2,6-i-Pr2C6H3))2)AlH2] (278608-73-4) + (CH3)2(C3HN2Ge)(2,6-iPr2C6H3)2OCHO (1109286-34-1) → (CH3)2(C3HN2Ge)(2,6-iPr2C6H3)2OCHO (1594135-97-3)

Guidance literature:

In toluene; at -50 - 20 ℃; for 12h; Inert atmosphere; Schlenk technique; Glovebox;

DOI:10.1039/c3dt53321b

upstream raw materials:

[C₃H(CH₃)2(N(2,6-diisopropylphenyl))2 chlorogermylene]

Downstream raw materials:

(HC(CMeNC-2,6-i-Pr₂C₆H₃)2)-germanium(II) hydride

lithium formate

deuteromethanol

(CH₃)2(C₃HN₂Ge)(2,6-iPr₂C₆H₃)2OCHO

Refernces