1-benzylbut-3-enyl methacrylate

Base Information

• Chemical Name: 1-benzylbut-3-enyl methacrylate
• CAS No.: 949171-58-8
• Molecular Formula: C₁₅H₁₈O₂
• Molecular Weight: 230.307
• Mol file: 949171-58-8.mol

Synonyms:1-benzylbut-3-enyl methacrylate

Chemical Property of 1-benzylbut-3-enyl methacrylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-benzylbut-3-enyl methacrylate

There total 2 articles about 1-benzylbut-3-enyl methacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

1-phenylpent-4-en-2-ol (61077-65-4) + Methacryloyl chloride (920-46-7,26937-45-1) → 1-benzylbut-3-enyl methacrylate (949171-58-8)

Guidance literature:

With triethylamine; In dichloromethane; for 2h;

DOI:10.1021/jo070600h

Reference yield:

phenylacetaldehyde (122-78-1) → 1-benzylbut-3-enyl methacrylate (949171-58-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / tetrahydrofuran / 4 h

2: 73 percent / Et₃N / CH₂Cl₂ / 2 h

With triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/jo070600h

Reference yield: 49.0%

1-benzylbut-3-enyl methacrylate (949171-58-8) → 6-benzyl-3-methyl-5,6-dihydro-2H-pyran-2-one

Guidance literature:

tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 20h; Heating;

DOI:10.1021/jo070600h

upstream raw materials:

1-phenylpent-4-en-2-ol

Methacryloyl chloride

phenylacetaldehyde

Refernces