Technology Process of C40H40N10O11
There total 4 articles about C40H40N10O11 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine; methanesulfonyl chloride / 2.5 h / 0 - 20 °C / Inert atmosphere
1.2: 2 h / 90 °C / Inert atmosphere
2.1: pyridine; ammonium hydroxide; triphenylphosphine / 20 °C / Inert atmosphere
3.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 336 h / 37 °C / Inert atmosphere
With
pyridine; ammonium hydroxide; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
N,N-dimethyl-formamide;
2.1: |Staudinger Azide Reduction;
DOI:10.1016/j.bmcl.2012.09.052
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine; ammonium hydroxide; triphenylphosphine / 20 °C / Inert atmosphere
2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 336 h / 37 °C / Inert atmosphere
With
pyridine; ammonium hydroxide; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
N,N-dimethyl-formamide;
1: |Staudinger Azide Reduction;
DOI:10.1016/j.bmcl.2012.09.052
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine / 0.08 h / 20 °C / Inert atmosphere
2.1: pyridine; methanesulfonyl chloride / 2.5 h / 0 - 20 °C / Inert atmosphere
2.2: 2 h / 90 °C / Inert atmosphere
3.1: pyridine; ammonium hydroxide; triphenylphosphine / 20 °C / Inert atmosphere
4.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 336 h / 37 °C / Inert atmosphere
With
pyridine; ammonium hydroxide; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
N,N-dimethyl-formamide;
3.1: |Staudinger Azide Reduction;
DOI:10.1016/j.bmcl.2012.09.052