PERFLUOROMETHYLVINYLETHER

Base Information

• Chemical Name: PERFLUOROMETHYLVINYLETHER
• CAS No.: 3823-94-7
• Molecular Formula: C₃H₃F₃O
• Molecular Weight: 112.051
• Hs Code.: 2909199090
• Mol file: 3823-94-7.mol

Synonyms:methyl 1,2,2-trifluorovinyl ether;trifluoro-methoxy-ethene;PERFLUOROMETHYLVINYLETHER;methyl trifluorovinyl ether;1,1,2-trifluoro-2-methoxyethene;

Chemical Property of PERFLUOROMETHYLVINYLETHER

Chemical Property:

• PSA: 9.23000
• LogP: 4.34380

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s): 3
• Hazard Codes: 3

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of PERFLUOROMETHYLVINYLETHER

There total 3 articles about PERFLUOROMETHYLVINYLETHER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium benzoate (532-32-1) + Sodium; 2,3,3,3-tetrafluoro-2-methoxy-propionate (123202-05-1) → benzoic acid methyl ester (93-58-3,5705-52-2,80226-58-0) + trifluoroacetic acid-methyl ester (431-47-0) + methyl 3,3,3-trifluoropyruvate (13089-11-7) + methyl 1,2,2-trifluorovinyl ether (3823-94-7) + benzoyl fluoride (455-32-3) + 2-fluoro-2-methoxy trifluoropropanoic acid methyl ester (10186-63-7)

Guidance literature:

at 230 ℃; for 1.75h; under 0.01 Torr; Product distribution; Mechanism;

DOI:10.1016/S0022-1139(00)80362-0

Reference yield:

Potassium; 2,3,3,3-tetrafluoro-2-methoxy-propionate (129880-35-9) → Methyl fluoride (593-53-3) + trifluoroacetic acid-methyl ester (431-47-0) + methyl 1,2,2-trifluorovinyl ether (3823-94-7) + 2-fluoro-2-methoxy trifluoropropanoic acid methyl ester (10186-63-7) + α-methoxytetrafluoropropionyl fluoride (85036-47-1)

Guidance literature:

at 250 ℃; for 1.5h; under 0.01 Torr; Product distribution; Mechanism;

DOI:10.1016/S0022-1139(00)80362-0

Reference yield:

Caesium; 2,3,3,3-tetrafluoro-2-methoxy-propionate (129880-36-0) → Carbonyl fluoride (353-50-4) + trifluoroacetyl fluoride (354-34-7) + methyl 1,2,2-trifluorovinyl ether (3823-94-7) + 2-fluoro-2-methoxy trifluoropropanoic acid methyl ester (10186-63-7) + α-methoxytetrafluoropropionyl fluoride (85036-47-1) + trifluoroacetic anhydride (407-25-0)

Guidance literature:

at 250 ℃; for 1.5h; under 0.01 Torr; Product distribution; Mechanism;

DOI:10.1016/S0022-1139(00)80362-0

upstream raw materials:

Caesium; 2,3,3,3-tetrafluoro-2-methoxy-propionate

Potassium; 2,3,3,3-tetrafluoro-2-methoxy-propionate

sodium benzoate

Sodium; 2,3,3,3-tetrafluoro-2-methoxy-propionate

Downstream raw materials:

1,1,2,2-Tetrafluoro-1-methoxy-2-nitroso-ethane

Bis(trifluoromethyl)disulfid

1,2-dichloro-1,1,2-trifluoro-2-methoxyethane

1,2,2-Trifluor-2-chlor-1-methoxy-1--aethan

Refernces