ethyl (4-methoxyphenyl)carbamodithioate

Base Information

• Chemical Name: ethyl (4-methoxyphenyl)carbamodithioate
• CAS No.: 56134-95-3
• Molecular Formula: C₁₀H₁₃NOS₂
• Molecular Weight: 227.351
• Mol file: 56134-95-3.mol

Synonyms:ethyl (4-methoxyphenyl)carbamodithioate

Chemical Property of ethyl (4-methoxyphenyl)carbamodithioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl (4-methoxyphenyl)carbamodithioate

There total 1 articles about ethyl (4-methoxyphenyl)carbamodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

carbon disulfide (75-15-0,12122-00-8) + 4-methoxy-aniline (104-94-9) → ethyl (4-methoxyphenyl)carbamodithioate (56134-95-3)

Guidance literature:

carbon disulfide; 4-methoxy-aniline; In ethanol; water; for 2h; Cooling with ice; Green chemistry;

ethyl halide; In ethanol; water; at 20 ℃; Cooling with ice; Green chemistry;

DOI:10.1007/s11164-017-3167-1

Reference yield: 100.0%

ammonium hydroxide (1336-21-6) + ethyl (4-methoxyphenyl)carbamodithioate (56134-95-3) → 1-(4-methoxyphenyl)thiourea (2293-07-4)

Guidance literature:

at 60 ℃; Neat (no solvent);

DOI:10.1016/j.tetlet.2008.10.063

Reference yield: 100.0%

ethyl (4-methoxyphenyl)carbamodithioate (56134-95-3) + diethylamine (109-89-7) → N,N-diethyl-N'-(4-methoxy-phenyl)-thiourea

Guidance literature:

at 60 ℃; Neat (no solvent);

DOI:10.1016/j.tetlet.2008.10.063

upstream raw materials:

carbon disulfide

4-methoxy-aniline

Downstream raw materials:

N-(4-methoxyphenyl)-N’-piperidinethiourea

morpholine-4-carbothioic acid 4-methoxyphenylamide

1-(4-methoxyphenyl)thiourea

C₁₂H₁₈N₂OS

Refernces