C₂₁H₂₃FOSSi

Base Information

• Chemical Name: C₂₁H₂₃FOSSi
• CAS No.: 1007388-26-2
• Molecular Formula: C₂₁H₂₃FOSSi
• Molecular Weight: 370.563
• Mol file: 1007388-26-2.mol

Synonyms:C₂₁H₂₃FOSSi

Chemical Property of C₂₁H₂₃FOSSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₂₁H₂₃FOSSi

There total 1 articles about C₂₁H₂₃FOSSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

((4-bromothiophen-2-yl)methoxy)(tert-butyl)diphenylsilane (1007388-25-1) → C21H23FOSSi (1007388-27-3) + C21H23FOSSi (1007388-26-2)

Guidance literature:

((4-bromothiophen-2-yl)methoxy)(tert-butyl)diphenylsilane; With n-butyllithium; In tetrahydrofuran; hexanes; at -78 ℃; for 1h;

With N-fluorobis(benzenesulfon)imide; In tetrahydrofuran; hexanes; at -78 - 20 ℃;

With water; ammonium chloride; In tetrahydrofuran; hexanes;

Reference yield:

C21H23FOSSi (1007388-27-3) + C21H23FOSSi (1007388-26-2) → (5-fluorothiophen-2-yl)methanol (824983-56-4) + (4-fluorothiophen-2-yl)methanol (1007388-28-4)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 25 ℃; for 16h;

upstream raw materials:

((4-bromothiophen-2-yl)methoxy)(tert-butyl)diphenylsilane

Downstream raw materials:

(5-fluorothiophen-2-yl)methanol

(4-fluorothiophen-2-yl)methanol

Refernces