Technology Process of N,N'-bis<3-<(benzyloxycarbonyl)amino>propyl>-3-pentanediamide
There total 3 articles about N,N'-bis<3-<(benzyloxycarbonyl)amino>propyl>-3-pentanediamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diethyl cyanophosphonate; triethylamine;
In
N,N-dimethyl-formamide;
1.) 20 deg C, 1 h, 2.) 100 deg C, 30 min;
DOI:10.1021/jm00151a011
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 39 percent / KHCOO3 / H2O; bis-(2-methoxy-ethyl) ether / 4 h / 20 °C
2: 72 percent / diethyl phosphorocyanidate, Et3N / dimethylformamide / 1.) 20 deg C, 1 h, 2.) 100 deg C, 30 min
With
diethyl cyanophosphonate; potassium hydrogencarbonate; triethylamine;
In
diethylene glycol dimethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00151a011
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 39 percent / KHCOO3 / H2O; bis-(2-methoxy-ethyl) ether / 4 h / 20 °C
2: 72 percent / diethyl phosphorocyanidate, Et3N / dimethylformamide / 1.) 20 deg C, 1 h, 2.) 100 deg C, 30 min
With
diethyl cyanophosphonate; potassium hydrogencarbonate; triethylamine;
In
diethylene glycol dimethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00151a011
