2-furyl-di(c-hexyl)phosphine oxide

Base Information

• Chemical Name: 2-furyl-di(c-hexyl)phosphine oxide
• CAS No.: 1415212-06-4
• Molecular Formula: C₁₆H₂₅O₂P
• Molecular Weight: 280.347
• Mol file: 1415212-06-4.mol

Synonyms:2-furyl-di(c-hexyl)phosphine oxide

Chemical Property of 2-furyl-di(c-hexyl)phosphine oxide

Chemical Property:

Purity/Quality:

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Technology Process of 2-furyl-di(c-hexyl)phosphine oxide

There total 2 articles about 2-furyl-di(c-hexyl)phosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-iodofuran (54829-48-0) + dicyclohexylphosphine oxide (14717-29-4) → 2-furyl-di(c-hexyl)phosphine oxide (1415212-06-4)

Guidance literature:

With copper(l) iodide; potassium carbonate; triphenylphosphine; In toluene; at 110 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.tet.2012.10.064

Reference yield: 75.0%

dicyclohexylphosphine oxide (14717-29-4) + C11H10O4S → 2-furyl-di(c-hexyl)phosphine oxide (1415212-06-4)

Guidance literature:

With pyridine; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 1-[2-(di-tert-butylphosphanyl)phenyl]-4-methoxy-piperidine; In tetrahydrofuran; toluene; at 50 ℃; Inert atmosphere; Glovebox; Sealed tube;

DOI:10.1177/1747519821994533

upstream raw materials:

2-iodofuran

dicyclohexylphosphine oxide

Refernces

• 1、 Stankevi?, Marek,W?odarczyk, Adam. "Efficient copper(I)-catalyzed coupling of secondary phosphine oxides with aryl halides". . p. 73 - 81. Retrieved 2013/01/15.