Technology Process of 8-Sulfanylquinoline-4-carboxylic acid
There total 4 articles about 8-Sulfanylquinoline-4-carboxylic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
water;
for 12h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydroxide / water / 0.17 h / 110 °C / Microwave irradiation
2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 150 °C
3: hydrogenchloride / water / 12 h / Reflux
With
hydrogenchloride; sodium hydride; sodium hydroxide;
In
water; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diphenylether / 4 h / 20 - 250 °C
2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 150 °C
3: hydrogenchloride / water / 12 h / Reflux
With
hydrogenchloride; sodium hydride;
In
diphenylether; water; N,N-dimethyl-formamide; mineral oil;