5-chlorosalicylaldehyde azine

Base Information

• Chemical Name: 5-chlorosalicylaldehyde azine
• CAS No.: 903635-16-5
• Molecular Formula: C₁₄H₁₁ClN₂O₂
• Molecular Weight: 274.707
• Mol file: 903635-16-5.mol

Synonyms:5-chlorosalicylaldehyde azine

Chemical Property of 5-chlorosalicylaldehyde azine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-chlorosalicylaldehyde azine

There total 2 articles about 5-chlorosalicylaldehyde azine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

2-(hydrazonomethyl)phenol (3291-00-7) + 5-chlorosalicyclaldehyde (635-93-8) → 5-chlorosalicylaldehyde azine (903635-16-5)

Guidance literature:

In ethanol; at 20 ℃;

DOI:10.1016/j.dyepig.2014.04.020

Reference yield:

2-(2',4'-dinitrobenzenesulfonyl)-5-chlorosalicylaldehyde azine (1613187-95-3) + 2-mercapto-5-methyl-1,3,4-thiadiazole (29490-19-5) → 5-chlorosalicylaldehyde azine (903635-16-5) + C9H6N4O4S2 (353256-57-2) + sulfur dioxide (7446-09-5,12143-17-8,89125-89-3)

Guidance literature:

at 37 ℃; for 0.5h; pH=7.4; Alkaline conditions;

DOI:10.1039/c8tb00414e

upstream raw materials:

2-(hydrazonomethyl)phenol

5-chlorosalicyclaldehyde

2-(2',4'-dinitrobenzenesulfonyl)-5-chlorosalicylaldehyde azine

2-mercapto-5-methyl-1,3,4-thiadiazole

Refernces

• 1、 Peng, Lu,Zhou, Zhaojuan,Wei, Ruirui,Li, Kai,Song, Panshu,Tong, Aijun. "A fluorescent probe for thiols based on aggregation-induced emission and its application in live-cell imaging". . p. 24 - 31. Retrieved 2014/05/20.